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Treatment of [CB<jats:sub>11<\/jats:sub>H<jats:sub>11<\/jats:sub>\u201012\u2010C\u2261CH]<jats:sup>\u2212<\/jats:sup> with CuI and ammonia affords {(CB<jats:sub>11<\/jats:sub>H<jats:sub>11<\/jats:sub>\u201012\u2010C\u2261C)<jats:sub>2<\/jats:sub>Cu<jats:sub>4<\/jats:sub>(NH<jats:sub>3<\/jats:sub>)<jats:sub>3<\/jats:sub>}<jats:sub><jats:italic>n<\/jats:italic><\/jats:sub> (<jats:bold>2<\/jats:bold>). Addition of selected phosphine and pyridine ligands transforms <jats:bold>2<\/jats:bold> to a range of homometallic products <jats:bold>3<\/jats:bold>\u2013<jats:bold>13<\/jats:bold>. All compounds have been characterized by X\u2010ray crystallography, which reveals a surprising variety of structural complexity featuring cores with two to ten Cu<jats:sup>+<\/jats:sup> centers. In the solid state, products <jats:bold>3<\/jats:bold>\u2013<jats:bold>13<\/jats:bold> exhibit room\u2010temperature phosphorescence across the visible spectrum in colors from blue to deep red. Lifetimes at room temperature are in the microsecond regime, and quantum yields of up to \u03a6=0.99 are observed.<\/jats:p>","DOI":"10.1002\/chem.201900584","type":"journal-article","created":{"date-parts":[[2019,3,31]],"date-time":"2019-03-31T22:11:58Z","timestamp":1554070318000},"page":"8754-8759","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":27,"title":["Atomically Defined Monocarborane Copper(I) Acetylides with Structural and Luminescence Properties Tuned by Ligand Sterics"],"prefix":"10.1002","volume":"25","author":[{"given":"Kang","family":"Zhang","sequence":"first","affiliation":[{"name":"Department of Chemistry Zhejiang University  38 Zheda Road 310027 Hangzhou P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yunjun","family":"Shen","sequence":"additional","affiliation":[{"name":"Department of Chemistry Zhejiang University  38 Zheda Road 310027 Hangzhou P. R. 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