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However, trapping the transient aryllithiums in a \u201chalogen dance\u201d is still challenging. Herein is reported the trapping of such short\u2010lived azolyllithiums in a batch reactor by developing a finely tuned in\u2005situ zincation using zinc halide diamine complexes. The reaction rate is controlled by the appropriate choice of diamine ligand. The reaction is operationally simple and can be performed at 0\u2009\u00b0C with high reproducibility on a multigram scale. 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