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While for As both HAs=CH<jats:sub>2<\/jats:sub>, As\u2212CH<jats:sub>3<\/jats:sub> and the methylene compound As=CH<jats:sub>2<\/jats:sub> are identified in the spectrum, the only Sb compound observed is Sb\u2212CH<jats:sub>3<\/jats:sub>. Thus, there is a step in the main group\u200515 between As and Sb, regarding the relative stability of the methyl compounds. Ionisation energies, vibrational frequencies and spin\u2010orbit splittings were determined for the methyl compound from photoion mass\u2010selected photoelectron spectra. Although the spectroscopic results for organoantimony resemble those for the previously investigated bismuth compounds, EPR spectroscopic experiments indicate a far lower tendency for methyl transfer for Sb(CH<jats:sub>3<\/jats:sub>)<jats:sub>3<\/jats:sub> compared to Bi(CH<jats:sub>3<\/jats:sub>)<jats:sub>3<\/jats:sub>. This study concludes investigations on low\u2010valent organopnictogen compounds.<\/jats:p>","DOI":"10.1002\/chem.202300637","type":"journal-article","created":{"date-parts":[[2023,3,30]],"date-time":"2023-03-30T11:38:22Z","timestamp":1680176302000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":6,"title":["Bonding in Low\u2010Coordinated Organoarsenic and Organoantimony Compounds: A Threshold Photoelectron Spectroscopic Investigation"],"prefix":"10.1002","volume":"29","author":[{"given":"Emil","family":"Karaev","sequence":"first","affiliation":[{"name":"Institute of Physical and Theoretical Chemistry Julius-Maximilians-Universit\u00e4t W\u00fcrzburg  Am Hubland 97074 W\u00fcrzburg Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Marius","family":"Gerlach","sequence":"additional","affiliation":[{"name":"Institute of Physical and Theoretical Chemistry Julius-Maximilians-Universit\u00e4t W\u00fcrzburg  Am Hubland 97074 W\u00fcrzburg Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Lukas","family":"Faschingbauer","sequence":"additional","affiliation":[{"name":"Institute of Physical and Theoretical Chemistry Julius-Maximilians-Universit\u00e4t W\u00fcrzburg  Am Hubland 97074 W\u00fcrzburg Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Jacqueline","family":"Ramler","sequence":"additional","affiliation":[{"name":"Department of Chemistry Philipps-University of Marburg  Hans-Meerwein-Str. 4 35032 Marburg Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Ivo","family":"Krummenacher","sequence":"additional","affiliation":[{"name":"Institute of Inorganic Chemistry University of W\u00fcrzburg  Am Hubland 97074 W\u00fcrzburg Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-0176-0939","authenticated-orcid":false,"given":"Crispin","family":"Lichtenberg","sequence":"additional","affiliation":[{"name":"Department of Chemistry Philipps-University of Marburg  Hans-Meerwein-Str. 4 35032 Marburg Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Patrick","family":"Hemberger","sequence":"additional","affiliation":[{"name":"Laboratory for Synchrotron Radiation and Femtochemistry Paul Scherrer Institut (PSI)  5232 Villigen Switzerland"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Ingo","family":"Fischer","sequence":"additional","affiliation":[{"name":"Institute of Physical and Theoretical Chemistry Julius-Maximilians-Universit\u00e4t W\u00fcrzburg  Am Hubland 97074 W\u00fcrzburg Germany"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2023,5,2]]},"reference":[{"key":"e_1_2_10_1_1","unstructured":"\u00a0"},{"key":"e_1_2_10_2_2","doi-asserted-by":"crossref","first-page":"8373","DOI":"10.1016\/S0040-4020(02)01000-1","volume":"58","author":"Leonard N. 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