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To overcome that limitation, an iso\u2010tellurazole <jats:italic>N<\/jats:italic>\u2010oxide was derivatized with a primary alcohol group; the compound is soluble in polar solvents and stable in acidic to neutral aqueous media. Nickel (II) and iron (II) form macrocyclic complexes with six molecules of that iso\u2010tellurazole <jats:italic>N<\/jats:italic>\u2010oxide in a hitherto not\u2010observed macrocyclic arrangement defined by CTe\u22c5\u22c5\u22c5O chalcogen bonds and \u03ba<jats:sup>6<\/jats:sup>\u2010O bound to the metal ion. 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