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In the bimetallic MOFs the ratio M:M\u2019 was 4\u2009:\u20091. The mono\u2010 and bimetallic MOFs were selected to systematically explore the catalytic\u2010activity of their derived metal oxide\/hydroxides for the oxygen evolution reaction (OER). Among all tested bimetallic MOF\u2010derived catalysts, the NiCoMOF exhibits superior catalytic activity for the OER with the lowest overpotentials of 301\u2005mV and Tafel slopes of 42\u2005mV\u2009dec<jats:sup>\u22121<\/jats:sup> on a rotating disk glassy carbon electrode (RD\u2010GCE) in 1\u2005mol\u2009L<jats:sup>\u22121<\/jats:sup> KOH electrolyte at a current density of 10\u2005mA\u2009cm<jats:sup>\u22122<\/jats:sup>. In addition, NiCoMOF was <jats:italic>insitu<\/jats:italic> grown in just 25\u2005min by the MW synthesis on the surface of nickel foam (NF) with, for example, a mass loading of 16.6 mg<jats:sub>MOF<\/jats:sub>\/g<jats:sub>NF<\/jats:sub>, where overpotentials of 313 and 328\u2005mV at current densities of 50 and 300\u2005mA\u2009cm<jats:sup>\u22122<\/jats:sup>, respectively, were delivered and superior long\u2010term stability for practical OER application. The low Tafel slope of 27\u2005mV\u2009dec<jats:sup>\u22121<\/jats:sup>, as well as a low reaction resistance from electrochemical impedance spectroscopy (EIS) measurement (R<jats:sub>far<\/jats:sub>=2 \u03a9), confirm the excellent OER performance of this NiCoMOF\/NF composite. During the electrocatalytic processes or even before upon KOH pre\u2010treatment, the MOFs are transformed to the mixed\u2010metal hydroxide phase \u03b1\u2010\/\u03b2\u2010M(OH)<jats:sub>2<\/jats:sub> which presents the active species in the reactions (turnover frequency TOF=0.252\u2005s<jats:sup>\u22121<\/jats:sup> at an overpotential of 320\u2005mV). Compared to the TOF from \u03b2\u2010M(OH)<jats:sub>2<\/jats:sub> (0.002\u2005s<jats:sup>\u22121<\/jats:sup>), our study demonstrates that a bimetallic MOF improves the electrocatalytic performance of the derived catalyst by giving an intimate and uniform mixture of the involved metals at the nanoscale.<\/jats:p>","DOI":"10.1002\/chem.202401644","type":"journal-article","created":{"date-parts":[[2024,6,13]],"date-time":"2024-06-13T09:33:04Z","timestamp":1718271184000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":16,"title":["Microwave\u2010Assisted Ultrafast Synthesis of Bimetallic Nickel\u2010Cobalt Metal\u2010Organic Frameworks for Application in the Oxygen Evolution Reaction"],"prefix":"10.1002","volume":"30","author":[{"given":"Thi Hai Yen","family":"Beglau","sequence":"first","affiliation":[{"name":"Institut f\u00fcr Anorganische Chemie und Strukturchemie Heinrich-Heine-Universit\u00e4t D\u00fcsseldorf  40204 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