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In the presence of two additional sodium ions, a unique molecular architecture, with triple combination of ligands (cyclic and acyclic silsesquioxanes as well as acetates), has been formed. The structure was established by single\u2010crystal X\u2010ray diffraction based on the use of synchrotron radiation. Complex\n                    <jats:bold>1<\/jats:bold>\n                    was evaluated as precatalyst in the Baeyer\u2013Villiger oxidation of cyclohexanone towards \u03f5\u2010caprolactone, employing hydrogen peroxide,\n                    <jats:italic>tert<\/jats:italic>\n                    \u2010butyl hydroperoxide (TBHP) or\n                    <jats:italic>m<\/jats:italic>\n                    \u2010chloroperoxybenzoic acid (mCPBA) as oxidants, in an aqueous acidic acetonitrile medium. The direct formation of the lactone from cyclohexane\n                    <jats:italic>via<\/jats:italic>\n                    a tandem peroxidative oxidation\/Baeyer\u2013Villiger oxidation was also studied. For both substrates, the best results (\u03f5\u2010caprolactone yields up to 100\u2009% or 26\u2009%, from cyclohexanone or cyclohexane, respectively) were achieved with mCPBA under considerably mild conditions,\n                    <jats:italic>i.\u2009e<\/jats:italic>\n                    ., conventional heating at 50\u2009\u00b0C for 4\u2005h or microwave (MW) irradiation at 80\u2009\u00b0C for only 30\u2005minutes.\n                  <\/jats:p>","DOI":"10.1002\/chem.202403604","type":"journal-article","created":{"date-parts":[[2024,12,10]],"date-time":"2024-12-10T06:54:56Z","timestamp":1733813696000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":8,"title":["Combination of Phenylsilsesquioxane and Acetate Ligands as an Approach to a Record High Nuclear Cu\n                    <sub>13<\/sub>\n                    Na\n                    <sub>2<\/sub>\n                    \u2010Cage. Synthesis, Unique Structure, and Catalytic Activity"],"prefix":"10.1002","volume":"31","author":[{"ORCID":"https:\/\/orcid.org\/0000-0003-3136-3675","authenticated-orcid":false,"given":"Alexey N.","family":"Bilyachenko","sequence":"first","affiliation":[{"name":"A.\u2005N. 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Nesmeyanov Institute of Organoelement Compounds Russian Academy of Sciences  28 Vavilov Street 119334 Moscow Russian Federation"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-1954-2809","authenticated-orcid":false,"given":"Nikolai N.","family":"Lobanov","sequence":"additional","affiliation":[{"name":"Peoples' Friendship University of Russia (RUDN University)  6 Miklukho-Maklaya Street Moscow 117198 Russian Federation"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8315-3501","authenticated-orcid":false,"given":"Zhi","family":"Wang","sequence":"additional","affiliation":[{"name":"Key Lab of Colloid and Interface Chemistry Ministry of Education School of Chemistry and Chemical Engineering Shandong University  Jinan Shandong 250100 China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-9658-4105","authenticated-orcid":false,"given":"Karim","family":"Ragimov","sequence":"additional","affiliation":[{"name":"Baku State University  Z. 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