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Therefore, their neutralisation requires harsh oxidation conditions, but also precise selectivity. Here we report the safe and effective detoxification of surrogates CEES and PhX by selective oxidation of the sulfur atom by generating peracetic acid from AcOEt and aq. H<jats:sub>2<\/jats:sub>O<jats:sub>2<\/jats:sub> assisted by the supported lipase CALB. 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