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It offers a comprehensive report on the fabrication of ZnS\u2500CuSe nanocomposites with varying compositions (90, 70, and 50% ZnS combined with 10, 30, and 50% CuSe), denoted as CZ\u20101, CZ\u20102, and CZ\u20103, via a wet\u2010chemical method. Comprehensive characterization was conducted to assess phase purity, structural integrity, composition, detection of free radicals, and optical properties. The results revealed that the average crystallite sizes of ZnS and CuSe were 46.91 and 20.31 nm, respectively. Morphological analysis showed CuSe formed nanoflakes, whereas ZnS appeared as nanoparticles. Optical properties revealed a red shift in absorption spectra and a decrease in band gap with increasing CuSe concentration. Electrons in the CBM (conduction band minimum) can be captured by \u2022O\n                    <jats:sub>2<\/jats:sub>\n                    to produce large amounts of \u2022O\n                    <jats:sub>2<\/jats:sub>\n                    \u2010 and \u2022OH radicals, formed via \u2022O\n                    <jats:sub>2<\/jats:sub>\n                    \u2010 \u2192H\n                    <jats:sub>2<\/jats:sub>\n                    O\n                    <jats:sub>2<\/jats:sub>\n                    \u2192\u2022OH. DFT calculations support these findings, offering insights into how CuSe affects the electronic structure of ZnS. Among the materials, CZ\u20103 showed superior photocatalytic activity, achieving 98% degradation of methylene blue (MB) dye and effective inhibition of B. subtilis and P. aeruginosa under visible light irradiation.\n                  <\/jats:p>","DOI":"10.1002\/chem.202404050","type":"journal-article","created":{"date-parts":[[2025,3,24]],"date-time":"2025-03-24T16:58:22Z","timestamp":1742835502000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["Enhancing Photocatalytic and Antibacterial Properties Through a Synergistic Approach in ZnS\u2013CuSe Nanocomposites"],"prefix":"10.1002","volume":"31","author":[{"ORCID":"https:\/\/orcid.org\/0009-0007-6012-5648","authenticated-orcid":false,"given":"Syed Awais","family":"Ahmad","sequence":"first","affiliation":[{"name":"College of Physics and Electronics Information, Yunnan Key Laboratory of Opto\u2010Electronic Information Technology, Key Laboratory of Advanced Technique &amp; Preparation for Renewable Energy Materials\u2010Ministry of Education Yunnan Normal University  Kunming People's Republic of China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Rui","family":"Bao","sequence":"additional","affiliation":[{"name":"Postoperative Intensive Care Unit, Yunnan Fuwai Cardiovascular Hospital  Kunming People's Republic of China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Muhammad","family":"Arif","sequence":"additional","affiliation":[{"name":"Qingdao Key Laboratory of Materials for Tissue Repair and Rehabilitation, Shandong Engineering Research Center for Tissue Rehabilitation Materials and Devices, School of Rehabilitation Sciences and Engineering Qingdao Hospital University of Health and Rehabilitation Sciences (Qingdao Municipal Hospital)  Qingdao People's Republic of China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Muhammad","family":"Awais","sequence":"additional","affiliation":[{"name":"Department of Physics COMSATS University Islamabad  Islamabad Pakistan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yingkai","family":"Liu","sequence":"additional","affiliation":[{"name":"College of Physics and Electronics Information, Yunnan Key Laboratory of Opto\u2010Electronic Information Technology, Key Laboratory of Advanced Technique &amp; Preparation for Renewable Energy Materials\u2010Ministry of Education Yunnan Normal University  Kunming People's Republic of China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6859-5683","authenticated-orcid":false,"given":"Hong\u2010En","family":"Wang","sequence":"additional","affiliation":[{"name":"College of Physics and Electronics Information, Yunnan Key Laboratory of Opto\u2010Electronic Information Technology, Key Laboratory of Advanced Technique &amp; Preparation for Renewable Energy Materials\u2010Ministry of Education Yunnan Normal University  Kunming People's Republic of China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Weibin","family":"Zhang","sequence":"additional","affiliation":[{"name":"College of Physics and Electronics Information, Yunnan Key Laboratory of Opto\u2010Electronic Information Technology, Key Laboratory of Advanced Technique &amp; Preparation for Renewable Energy Materials\u2010Ministry of Education Yunnan Normal University  Kunming People's Republic of China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2025,4,13]]},"reference":[{"key":"e_1_2_10_1_1","doi-asserted-by":"publisher","DOI":"10.1021\/acsomega.3c00198"},{"key":"e_1_2_10_1_2","doi-asserted-by":"publisher","DOI":"10.1016\/j.surfin.2024.105039"},{"key":"e_1_2_10_2_1","doi-asserted-by":"publisher","DOI":"10.1021\/acsanm.0c02199"},{"key":"e_1_2_10_3_1","doi-asserted-by":"publisher","DOI":"10.1021\/acsanm.7b00242"},{"key":"e_1_2_10_3_2","doi-asserted-by":"publisher","DOI":"10.1016\/j.matpr.2023.06.381"},{"key":"e_1_2_10_4_1","doi-asserted-by":"publisher","DOI":"10.1021\/acsomega.3c00198"},{"key":"e_1_2_10_4_2","doi-asserted-by":"publisher","DOI":"10.1016\/j.surfin.2022.102249"},{"key":"e_1_2_10_5_1","doi-asserted-by":"publisher","DOI":"10.1080\/1040-840291046669"},{"key":"e_1_2_10_6_1","unstructured":"J. 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