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CPs\n                    <jats:bold>1<\/jats:bold>\n                    \u2013\n                    <jats:bold>3<\/jats:bold>\n                    all adopt similar two\u2010dimensional (2D) ring\u2010and\u2010rod layer structures, described as topologically 4\u2010connected 2\u2009\u22c5\u20096\n                    <jats:sup>5<\/jats:sup>\n                    nets where the Zn(II) centers act as 4\u2010connected nodes. CPs\n                    <jats:bold>1<\/jats:bold>\n                    and\n                    <jats:bold>2<\/jats:bold>\n                    are a pair of solvent\u2010mediated supramolecular isomers where the former shows a two\u2010fold interlocked 2D \u21922D polyrotaxane\u2010like entangled net and the latter reveals a four\u2010fold interpenetrated 2D \u21923D polyrotaxane entanglement. CP\n                    <jats:bold>3<\/jats:bold>\n                    is structure analgue of\n                    <jats:bold>1<\/jats:bold>\n                    . The formation of\n                    <jats:bold>1<\/jats:bold>\n                    \u2013\n                    <jats:bold>3<\/jats:bold>\n                    implies the realization of interpenetration control and supramolecular isomerism in polyrotaxanes by fine\u2010tuning the solvent compositions and ligand steric\u2010modulation. CPs\n                    <jats:bold>1<\/jats:bold>\n                    \u2013\n                    <jats:bold>3<\/jats:bold>\n                    all show high thermal stability approaching 400\u2009\u00b0C and good chemical stability in various solvents at room temperature for 24\u2005h. Further, CPs\n                    <jats:bold>1<\/jats:bold>\n                    \u2013\n                    <jats:bold>3<\/jats:bold>\n                    all are excellent turn\u2010off sensors to recognize Fe\n                    <jats:sup>3+<\/jats:sup>\n                    in water with high selectivity and sensitivity, great anti\u2010inference ability, and low limit of detection (LOD). The sensing mechanisms are found to be competitive absorption of excitation wavelength energy and\n                    <jats:styled-content>the occurrence of<\/jats:styled-content>\n                    framework\u2013Fe\n                    <jats:sup>3+<\/jats:sup>\n                    <jats:styled-content>interactions<\/jats:styled-content>\n                    .\n                  <\/jats:p>","DOI":"10.1002\/chem.202404336","type":"journal-article","created":{"date-parts":[[2025,1,19]],"date-time":"2025-01-19T22:36:28Z","timestamp":1737326188000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["Interpenetration Control in Metal\u2013Organic Polyrotaxanes via Solvent Composition and Ligand Steric\u2010Modulation: Supramolecular Isomerism and Luminescence Detection toward Fe\n                    <sup>3+<\/sup>\n                    Ions"],"prefix":"10.1002","volume":"31","author":[{"given":"Wei\u2010Ting","family":"Chen","sequence":"first","affiliation":[{"name":"Department of Applied Chemistry National Chi Nan University  Nantou 545 Taiwan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Meng\u2010Jung","family":"Tsai","sequence":"additional","affiliation":[{"name":"Department of Applied Chemistry National Chi Nan University  Nantou 545 Taiwan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Po\u2010Min","family":"Chuang","sequence":"additional","affiliation":[{"name":"Department of Applied Chemistry National Chi Nan University  Nantou 545 Taiwan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7257-4711","authenticated-orcid":false,"given":"Jing\u2010Yun","family":"Wu","sequence":"additional","affiliation":[{"name":"Department of Applied Chemistry National Chi Nan University  Nantou 545 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