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Despite the abundance and diversity of natural amino acids, their direct decarboxylation remains challenging. Here, we report the direct decarboxylation of amino acids to generate\n                    <jats:italic>\u03b1<\/jats:italic>\n                    \u2010aminocarbon radicals and their subsequent cross\u2010coupling, enabled by air\u2010stable nickel(0) complexes under photoexcitation without external photosensitizers. This mild catalytic system shows broad compatibility with diverse amino acids and aromatic functional groups, providing a new approach for their direct decarboxylation and functionalization.\n                  <\/jats:p>","DOI":"10.1002\/chem.71312","type":"journal-article","created":{"date-parts":[[2026,6,27]],"date-time":"2026-06-27T16:02:38Z","timestamp":1782576158000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["Photoexcited Nickel(0)\u2010Catalyzed Direct Decarboxylative Cross\u2010Coupling"],"prefix":"10.1002","volume":"32","author":[{"given":"Jingsheng","family":"Li","sequence":"first","affiliation":[{"name":"Key Laboratory of Applied Surface and Colloid Chemistry Ministry of Education and School of Chemistry and Chemical Engineering Shaanxi Normal University  Xi'an 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