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To date, avoiding the harsh mechanical force while achieving the synthesis of highly insoluble materials under mild, additive\u2010free, and solid\u2010state conditions remains a challenge especially if heterogeneous catalysis is considered. Inspired by the fundamental diffusion dynamics observed in nature, we developed a polymeric palladium\u2010catalyzed quasi\u2010solid\u2010state Suzuki\u2013Miyaura reaction that proceeds without mechanical input; that is, a granular motion of the components results from heat\u2010induced convection\u2010driven mass transfer. This approach enabled the synthesis of various polycyclic aromatic hydrocarbons and functional materials in up to 93% yields with Pd loadings as low as 500\u00a0mol ppm. Gram\u2010scale synthesis of dinaphthyl anthracene as a functional material was successfully achieved under the quasi\u2010solid\u2010state reaction conditions. Notably, since no mechanical force is applied during the reaction, it is well\u2010suited to be analyzed in real time, which is a challenge in solid\u2010state systems. As a result, in\u2010situ monitoring of the chemical changes of each of the solid reactants allowed the identification and real time monitoring of a boronate intermediate. In addition, direct microscopic visualization revealed changes in morphology and element distributions, proposing a granular motion mechanism for this transformation.<\/jats:p>","DOI":"10.1002\/chem.71429","type":"journal-article","created":{"date-parts":[[2026,7,22]],"date-time":"2026-07-22T21:22:19Z","timestamp":1784755339000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Heat\u2010Induced Granular Motion in Quasi\u2010Solid\u2010State Suzuki\u2013Miyaura Reaction"],"prefix":"10.1002","author":[{"given":"Bo\u0161ko","family":"Vrbica","sequence":"first","affiliation":[{"name":"RIKEN Center for Sustainable Resource Science (CSRS)  Wako Saitama Japan"},{"name":"Department of Chemical Science and Engineering Institute of Science Tokyo  Yokohama Japan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhenzhong","family":"Zhang","sequence":"additional","affiliation":[{"name":"RIKEN Center for Sustainable Resource Science (CSRS)  Wako Saitama Japan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Abhijit","family":"Sen","sequence":"additional","affiliation":[{"name":"RIKEN Center for Sustainable Resource Science (CSRS)  Wako Saitama Japan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Aya","family":"Ohno","sequence":"additional","affiliation":[{"name":"RIKEN Center for Sustainable Resource Science (CSRS)  Wako Saitama Japan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Daishi","family":"Inoue","sequence":"additional","affiliation":[{"name":"RIKEN Center for Emergent Matter Science (CEMS)  Wako Saitama Japan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Daisuke","family":"Hashizume","sequence":"additional","affiliation":[{"name":"RIKEN Center for Emergent Matter Science (CEMS)  Wako Saitama Japan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Nobutaka","family":"Maeda","sequence":"additional","affiliation":[{"name":"The Center for Energy Systems Design International Institute for Carbon\u2010Neutral Energy Research (WPI\u2010I2CNER) Kyushu University  Fukuoka Japan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tomoya","family":"Fukui","sequence":"additional","affiliation":[{"name":"Department of Chemical Science and Engineering Institute of Science Tokyo  Yokohama Japan"},{"name":"Laboratory for Chemistry and Life Science Institute of Integrated Research Institute of Science Tokyo  Yokohama Japan"},{"name":"Research Center for Autonomous Systems Materialogy (ASMat) Institute of Integrated Research Institute of Science Tokyo  Yokohama Japan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Takanori","family":"Fukushima","sequence":"additional","affiliation":[{"name":"Department of Chemical Science and Engineering Institute of Science Tokyo  Yokohama Japan"},{"name":"Laboratory for Chemistry and Life Science Institute of Integrated Research Institute of Science Tokyo  Yokohama Japan"},{"name":"Research Center for Autonomous Systems Materialogy (ASMat) Institute of Integrated Research Institute of Science Tokyo  Yokohama Japan"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3901-5926","authenticated-orcid":false,"given":"Yoichi M. 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