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DFT calculations show that \u2500SO\n                    <jats:sub>2<\/jats:sub>\n                    \u2500 bridges strongly increase the electrostatic surface potential (ESP) at lower rim CH sites. Receptors bearing two \u2500SO\n                    <jats:sub>2<\/jats:sub>\n                    \u2500 bridges at opposite corners and various upper rim substituents (H, Br, NO\n                    <jats:sub>2<\/jats:sub>\n                    ), and free OH groups were synthesized; NMR spectroscopy and single\u2010crystal X\u2010ray diffraction confirm cone conformations with inward\u2010oriented \u2500SO\n                    <jats:sub>2<\/jats:sub>\n                    \u2500 bridges. Anion binding studies with chloride in THF, THF:water, and chloroform show that replacing two \u2500CH\n                    <jats:sub>2<\/jats:sub>\n                    \u2500 bridges with \u2500SO\n                    <jats:sub>2<\/jats:sub>\n                    \u2500 bridges enhances CH binding by up to two orders of magnitude. Both CH and OH sites act as effective binding motifs, with their relative contributions governed by substituents and solvent. The solvent dependence arises from the distinct characterisation of the two sites: OH sites display highly localized positive ESPs, while CH sites possess more diffuse positive ESPs. THF selectively solvates OH sites whereas chloroform solvates CH sites while leaving OH binding intact. NMR, UV\u2013Vis, and ITC confirm distinct thermodynamic signatures for CH\u2010 and OH\u2010dominated complexes, establishing a solvent\u2010controlled hierarchy between the two motifs and enabling multisite receptors to remain effective across diverse environments.\n                  <\/jats:p>","DOI":"10.1002\/chem.71509","type":"journal-article","created":{"date-parts":[[2026,8,3]],"date-time":"2026-08-03T11:00:20Z","timestamp":1785754820000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Multisite Anion Receptors: Interplay of OH and CH Binding Sites in Sulfate\u2010Bridged Resorcinarenes"],"prefix":"10.1002","author":[{"ORCID":"https:\/\/orcid.org\/0009-0005-3927-5313","authenticated-orcid":false,"given":"Krzysztof J.","family":"Olender","sequence":"first","affiliation":[{"name":"Institute of Organic Chemistry Polish Academy of Sciences  Warsaw Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-0916-1575","authenticated-orcid":false,"given":"Marek P.","family":"Szyma\u0144ski","sequence":"additional","affiliation":[{"name":"Institute of Organic Chemistry Polish Academy of Sciences  Warsaw Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3653-2418","authenticated-orcid":false,"given":"Oksana","family":"Danylyuk","sequence":"additional","affiliation":[{"name":"Institute of Physical Chemistry Polish Academy of Sciences  Warsaw Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3869-1321","authenticated-orcid":false,"given":"Agnieszka","family":"Szumna","sequence":"additional","affiliation":[{"name":"Institute of Organic Chemistry Polish Academy of Sciences  Warsaw Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-7071-7125","authenticated-orcid":false,"given":"Esma R.","family":"Abdurakhmanova","sequence":"additional","affiliation":[{"name":"Institute of Organic Chemistry Polish Academy of Sciences  Warsaw Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2026,8,3]]},"reference":[{"key":"e_1_2_6_2_1","volume-title":"Supramolecular Chemistry","author":"Steed J. 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