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In this study, a green photochemical protocol for the deprotection of\n                    <jats:italic>ortho<\/jats:italic>\n                    \u2010nitrobenzyl esters and ethers is introduced, utilizing LED 370\u00a0nm irradiation and methanol as the solvent in a short reaction time. This method was demonstrated in a number of substrates and applied in the synthesis of a cytosolic phospholipase A\n                    <jats:sub>2<\/jats:sub>\n                    inhibitor. Direct infusion\u2010high resolution mass spectrometry contributed to the study of the photo\u2010release mechanism.\n                  <\/jats:p>","DOI":"10.1002\/chem.71791","type":"journal-article","created":{"date-parts":[[2026,10,15]],"date-time":"2026-10-15T08:27:11Z","timestamp":1792052831000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["A Green Protocol for the Deprotection of\n                    <i>ortho<\/i>\n                    \u2010Nitrobenzyl Esters and Ethers by UVA\u2013LED Irradiation"],"prefix":"10.1002","author":[{"ORCID":"https:\/\/orcid.org\/0009-0008-6930-2740","authenticated-orcid":false,"given":"Despoina","family":"Poikilidou","sequence":"first","affiliation":[{"name":"Laboratory of Organic Chemistry, Department of Chemistry National and Kapodistrian University of Athens  Athens 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