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However, the synthesis of these compounds generally lacks a convenient protocol and often relies on harsh conditions involving expensive noble metals, toxic solvents, or external oxidants. In this context, we herein propose a sustainable alternative: a mechanochemical activation of zero\u2010valent copper powder via ball milling, which enables an oxidant\u2010free C\u2013N coupling reaction between arylboronic acids and sulfoximines. This method features broad substrate compatibility, straightforward scalability, and the use of recyclable copper powder that retains high activity after recovery.<\/jats:p>","DOI":"10.1002\/chem.71827","type":"journal-article","created":{"date-parts":[[2026,10,23]],"date-time":"2026-10-23T03:41:42Z","timestamp":1792726902000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Oxidant\u2010Free Mechanochemical N\u2010Arylation of Sulfoximines Using Zero\u2010Valent Copper Powder and Arylboronic Acid"],"prefix":"10.1002","author":[{"given":"Tao","family":"Fang","sequence":"first","affiliation":[{"name":"Guizhou Provincial Key Laboratory of Innovation and Manufacturing for Pharmaceuticals School of Pharmacy Zunyi Medical University  Zunyi China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Tingting","family":"Fan","sequence":"additional","affiliation":[{"name":"Guizhou Provincial Key Laboratory of Innovation and Manufacturing for Pharmaceuticals School of Pharmacy Zunyi Medical University  Zunyi China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Cong","family":"Chen","sequence":"additional","affiliation":[{"name":"Guizhou Provincial Key Laboratory of Innovation and Manufacturing for Pharmaceuticals School of Pharmacy Zunyi Medical University  Zunyi China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhixiu","family":"Liu","sequence":"additional","affiliation":[{"name":"Guizhou Provincial Key Laboratory of Innovation and Manufacturing for Pharmaceuticals School of Pharmacy Zunyi Medical University  Zunyi China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-5693-5188","authenticated-orcid":false,"given":"Baodong","family":"Cui","sequence":"additional","affiliation":[{"name":"Guizhou Provincial Key Laboratory of Innovation and Manufacturing for Pharmaceuticals School of Pharmacy Zunyi Medical University  Zunyi China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1211-3486","authenticated-orcid":false,"given":"Yongzheng","family":"Chen","sequence":"additional","affiliation":[{"name":"Guizhou Provincial Key Laboratory of Innovation and Manufacturing for Pharmaceuticals School of Pharmacy Zunyi Medical University  Zunyi China"},{"name":"Key Laboratory of Basic Pharmacology of Ministry of Education, and Joint International Research Laboratory of Ethnomedicine of Ministry of Education Zunyi Medical University  Zunyi China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0005-6350-4120","authenticated-orcid":false,"given":"Shiming","family":"Zhang","sequence":"additional","affiliation":[{"name":"Guizhou Provincial Key Laboratory of Innovation and Manufacturing for Pharmaceuticals School of Pharmacy Zunyi Medical University  Zunyi China"},{"name":"Key Laboratory of Basic Pharmacology of Ministry of Education, and Joint International Research Laboratory of Ethnomedicine of Ministry of Education Zunyi Medical University  Zunyi China"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2026,10,22]]},"reference":[{"key":"e_1_2_7_2_1","doi-asserted-by":"crossref","first-page":"335","DOI":"10.1016\/j.trechm.2021.02.008","article-title":"Upscaling Mechanochemistry: Challenges and Opportunities for Sustainable Industry","volume":"3","author":"Colacino E.","year":"2021","journal-title":"Trends In Chemistry"},{"key":"e_1_2_7_3_1","doi-asserted-by":"crossref","first-page":"12342","DOI":"10.1021\/acssuschemeng.0c03942","article-title":"Catalytic Electrophilic C\u2013H Sulfenylation of Indoles With Disulfides Under Ball Milling","volume":"8","author":"Qin J.","year":"2020","journal-title":"ACS Sustainable Chemistry & Engineering"},{"key":"e_1_2_7_4_1","doi-asserted-by":"crossref","first-page":"910","DOI":"10.1021\/acssuschemeng.2c04720","article-title":"Piezocatalyzed Decarboxylative Acylation of Quinoxalin\u20102(1H)\u2010ones Using Ball Milling","volume":"11","author":"He Y.","year":"2023","journal-title":"ACS Sustainable Chemistry & Engineering"},{"issue":"19","key":"e_1_2_7_5_1","doi-asserted-by":"crossref","first-page":"6680","DOI":"10.1039\/D2CS00997H","article-title":"Green Metrics in Mechanochemistry","volume":"52","author":"Fantozzi N.","year":"2023","journal-title":"Chemical Society Reviews"},{"issue":"10","key":"e_1_2_7_6_1","doi-asserted-by":"crossref","first-page":"2145","DOI":"10.1002\/cssc.202100478","article-title":"Sustainability Assessment of Mechanochemistry by Using the Twelve Principles of Green Chemistry","volume":"14","author":"Ardila\u2010Fierro K. 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