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Divinylbenzene (DVB) and aliphatic monomers: ethylene glycol dimethacrylate (EGDMA) or N,N\u2032\u2010methylenebisacrylamide (NN) containing additional amide groups were used. The possibility of using the prepared copolymers (MMA\u2010NN, MMA\u2010EGDMA, MMA\u2010DVB) as adsorbents for the removal of toxic compounds such as dyes (C.I. Acid Red 18 (AR18), C.I. Acid Green 16 (AG16), C.I. Acid Violet 1 (AV1), C.I. Basic Yellow 2 (BY2), C.I. Basic Blue 3 (BB3) and C.I. Basic Red 46 (BR46)) and phenol (PhOH) from dye baths and effluents was evaluated. Preferential adsorption of basic\u2010type dyes compared to acid\u2010type dyes or phenol was observed by the polymers. Adsorbent based on MMA\u2010EGDMA exhibited the highest capacity for investigated dyes and phenol. The pseudo\u2010second order kinetic model as well as the intraparticle diffusion model can find application in predicting sorption kinetics. Based on the equilibrium sorption data fitted to the Langmuir, Freundlich, Temkin and Dubinin\u2010Radushkevich model, uptake of BB3, AV1 and PhOH is rather physisorption than chemisorption. The regeneration yield of MMA\u2010EGDMA does not exceed 60\u2009% using 1\u2005M HCl, 1\u2005M NaCl, and 1\u2005M NaOH in 50\u2009%v\/v methanol.<\/jats:p>","DOI":"10.1002\/cphc.202300719","type":"journal-article","created":{"date-parts":[[2023,10,29]],"date-time":"2023-10-29T23:14:20Z","timestamp":1698621260000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":6,"title":["New Methyl Methacrylate Derived Adsorbents \u2013 Synthesis, Characterization and Adsorptive Removal of Toxic Organic Compounds"],"prefix":"10.1002","volume":"25","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-5697-6075","authenticated-orcid":false,"given":"Monika","family":"Wawrzkiewicz","sequence":"first","affiliation":[{"name":"Department of Inorganic Chemistry Institute of Chemical Sciences, Faculty of Chemistry Maria Curie-Sklodowska University in  Lublin M. 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