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However, substantial electrostatic interactions between electron donors and acceptors induce polymer aggregation, limiting moldability and conductivity. In this study, robust donor polymers with high heat resistance were synthesized by bonding triphenylamine (TPA) derivatives and formaldehyde to phenolic groups. Resulting TPA\u2010based phenolic polymers exhibited flexible structures and fluorescence due to charge transfer with acceptor molecules. Furthermore, TPA\u2010based phenolic polymers\u2019 capacity to distinguish acceptor molecule sizes correlated with their molecular weight, reflecting upon donor\u2010acceptor interactions. 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