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Herein, ZnIn<jats:sub>2<\/jats:sub>S<jats:sub>4<\/jats:sub> hierarchical architectures assembled as ultrathin nanosheets were synthesized by a facile one\u2010pot polyol approach. Subsequently, the two\u2010dimensional\u2010network\u2010like MoSe<jats:sub>2<\/jats:sub> was successfully hybridized with ZnIn<jats:sub>2<\/jats:sub>S<jats:sub>4<\/jats:sub> by taking advantage of their analogous intrinsic layered morphologies. The noble\u2010metal\u2010free ZnIn<jats:sub>2<\/jats:sub>S<jats:sub>4<\/jats:sub>\/MoSe<jats:sub>2<\/jats:sub> heterostructures show enhanced photocatalytic H<jats:sub>2<\/jats:sub> evolution compared to pure ZnIn<jats:sub>2<\/jats:sub>S<jats:sub>4<\/jats:sub>. It is noteworthy that the optimum nanocomposite of ZnIn<jats:sub>2<\/jats:sub>S<jats:sub>4<\/jats:sub>\/2\u2009%\u2005MoSe<jats:sub>2<\/jats:sub> photocatalyst displays a high H<jats:sub>2<\/jats:sub> generation rate of 2228\u2005\u03bcmol\u2009g<jats:sup>\u22121<\/jats:sup>\u2009h<jats:sup>\u22121<\/jats:sup> and an apparent quantum yield (AQY) of 21.39\u2009% at 420\u2005nm. This study presents an unprecedented ZnIn<jats:sub>2<\/jats:sub>S<jats:sub>4<\/jats:sub>\/MoSe<jats:sub>2<\/jats:sub> metal\u2010sulfide\u2013metal\u2010selenide hybrid system for H<jats:sub>2<\/jats:sub> evolution. Importantly, the present efficient hybridization strategy reveals the potential of hierarchical nanoarchitectures for a multitude of energy storage and solar energy conversion applications.<\/jats:p>","DOI":"10.1002\/cssc.201701345","type":"journal-article","created":{"date-parts":[[2017,8,18]],"date-time":"2017-08-18T08:02:40Z","timestamp":1503043360000},"page":"4624-4631","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":162,"title":["Hierarchical ZnIn<sub>2<\/sub>S<sub>4<\/sub>\/MoSe<sub>2<\/sub> Nanoarchitectures for Efficient Noble\u2010Metal\u2010Free Photocatalytic Hydrogen Evolution under Visible Light"],"prefix":"10.1002","volume":"10","author":[{"given":"Deqian","family":"Zeng","sequence":"first","affiliation":[{"name":"Department of Materials Science and Engineering Collaborative Innovation Center of Chemistry for Energy Materials College of Materials Xiamen University  Xiamen 361005 P.R. 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