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Owing to their tunable structural properties, these materials are found to be useful for gas storage and separation technologies, as well as for catalytic applications. A cost\u2010effective zinc\u2010based MOF ([Zn(bpcda)(bdc)]<jats:sub><jats:italic>n<\/jats:italic><\/jats:sub>) is prepared by using <jats:italic>N<\/jats:italic>,<jats:italic>N<\/jats:italic>\u2032\u2010bis(pyridin\u20104\u2010ylmethylene)cyclohexane\u20101,4\u2010diamine [<jats:italic>N<\/jats:italic>,<jats:italic>N<\/jats:italic>\u2032\u2010bis(pyridin\u20104\u2010ylmethylene)cyclohexane\u20101,4\u2010diamine] and benzenedicarboxylic acid (bdc) linkers. This new material exhibits remarkable photoelectrochemical (PEC) catalytic activity in water splitting for the evolution of oxygen. Notably, this non\u2010noble metal\u2010based MOF, without requiring immobilization on other supports or containing metal particles, produced a highest photocurrent density of 31\u2005\u03bcA\u2009cm<jats:sup>\u22122<\/jats:sup> at 0.9\u2005V, with appreciable stability and negligible photocorrosion. Advantageously for the oxygen evolution process, no external reagents or sacrificial agents are required in the aqueous electrolyte solution.<\/jats:p>","DOI":"10.1002\/cssc.201702122","type":"journal-article","created":{"date-parts":[[2017,12,18]],"date-time":"2017-12-18T01:46:49Z","timestamp":1513561609000},"page":"542-546","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":24,"title":["Synthesis, Characterization, and Photoelectrochemical Catalytic Studies of a Water\u2010Stable Zinc\u2010Based Metal\u2013Organic Framework"],"prefix":"10.1002","volume":"11","author":[{"given":"Muhammad","family":"Altaf","sequence":"first","affiliation":[{"name":"Centre of Research Excellence in Nanotechnology (CENT) King Fahd University of Petroleum and Minerals  Dhahran 31261 Saudi Arabia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Manzar","family":"Sohail","sequence":"additional","affiliation":[{"name":"Centre of 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