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Transportation fuels are critical to economic development, globalization, and the advancement of society. Although ground vehicles and small aircraft are beginning a slow transition toward electric propulsion with energy sourced from solar radiation or wind, the extreme power requirements of jet aircraft require a more concentrated source of energy that is conveniently provided by liquid hydrocarbon fuels. This Review describes recent efforts to develop efficient routes for the conversion of crude biomass sources (e.\u2009g., lignocellulose) to cycloalkanes. These cycloalkanes impart advantageous properties to jet fuels, including increased density, higher volumetric heat of combustion, and enhanced operability. The combination of bio\u2010based cycloalkanes and synthetic paraffinic kerosenes allows for the preparation of 100\u2009% bio\u2010based fuels that can outperform conventional petroleum\u2010based fuels. In this Review methods are described that convert biomass\u2010derived small molecules, including furfural, furfuryl alcohol, 5\u2010hydroxymethylfurfural, cyclic ketones, phenolics, acyclic ketones, cyclic alcohols, furans, esters, and alkenes to high\u2010density cycloalkanes. In addition to describing the chemical transformations and catalysts that have been developed to efficiently produce various cycloalkanes, this Review includes summaries of key fuel properties, which highlight the ability to generate fuels with customized performance metrics. This work is intended to inspire other researchers to study the conversion of sustainable feedstocks to full\u2010performance aviation fuels. An acceleration of this research is critical to reducing the carbon footprint of commercial and military aviation on a timescale that will help blunt the impacts of global warming.<\/jats:p>","DOI":"10.1002\/cssc.202001641","type":"journal-article","created":{"date-parts":[[2020,8,28]],"date-time":"2020-08-28T09:07:35Z","timestamp":1598605655000},"page":"5777-5807","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":144,"title":["Bio\u2010Based Cycloalkanes: The Missing Link to High\u2010Performance Sustainable Jet Fuels"],"prefix":"10.1002","volume":"13","author":[{"given":"Jake A.","family":"Muldoon","sequence":"first","affiliation":[{"name":"US NAVY, NAWCWD Research Department, Chemistry Branch  China Lake, California 93555 USA"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2091-3539","authenticated-orcid":false,"given":"Benjamin G.","family":"Harvey","sequence":"additional","affiliation":[{"name":"US NAVY, NAWCWD Research Department, Chemistry Branch  China Lake, California 93555 USA"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2020,9,25]]},"reference":[{"key":"e_1_2_16_1_1","doi-asserted-by":"publisher","DOI":"10.1021\/ef101520v"},{"key":"e_1_2_16_2_1","volume-title":"Aviation Fuels Technical Review","author":"Bacha J.","year":"2000"},{"key":"e_1_2_16_3_1","doi-asserted-by":"publisher","DOI":"10.1021\/ef502618w"},{"key":"e_1_2_16_4_1","doi-asserted-by":"crossref","unstructured":"J. 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