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In\u2010situ catalytic transfer hydrogenation (CTH), using isopropanol and formic acid as solvent and in\u2010situ hydrogen sources, was demonstrated over metal\u2010doped and promoted MCM\u201041 for the depolymerization of oxygen\u2010rich (35.85\u2005wt%) lignin from Chinese fir sawdust (termed O\u2010lignin). A NiMo\/Al\u2010MCM\u201041 catalyst conferred an optimal lignin\u2010derived oil yield of 61.6\u2005wt% with a comparatively low molecular weight (\n                    <jats:italic>M<\/jats:italic>\n                    <jats:sub>w<\/jats:sub>\n                    =542\u2005g\u2009mol\n                    <jats:sup>\u22121<\/jats:sup>\n                    ,\n                    <jats:italic>M<\/jats:italic>\n                    <jats:sub>n<\/jats:sub>\n                    =290\u2005g mol\n                    <jats:sup>\u22121<\/jats:sup>\n                    ) and H\/C ratio of 1.39. High selectivity to alkyl guaiacols was attributed to efficient in\u2010situ hydrogen transfer from isopropanol\/formic acid donors, and a synergy between surface acid sites in the Al\u2010doped MCM\u201041 support and reducible Ni\/Mo species, which improved the chemical stability and quality of the resulting lignin\u2010derived bio\u2010oils.\n                  <\/jats:p>","DOI":"10.1002\/cssc.202200099","type":"journal-article","created":{"date-parts":[[2022,2,22]],"date-time":"2022-02-22T10:53:41Z","timestamp":1645527221000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":41,"title":["Selective Catalytic Transfer Hydrogenation of Lignin to Alkyl Guaiacols Over NiMo\/Al\u2010MCM\u201041"],"prefix":"10.1002","volume":"15","author":[{"given":"Xinyu","family":"Lu","sequence":"first","affiliation":[{"name":"Co-Innovation Center for Efficient Processing and Utilization of Forest Products, International Innovation Center for Forest Chemicals and Materials, College of Chemical Engineering Nanjing Forestry University  No. 159 Longpan Road Nanjing 210037 P. 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