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In this study, we detailed a simple colloidal\u2010based protocol for synthesizing a series of alloy nanoparticles with tuned Ni\/Co atomic ratios, thereby optimizing their electrochemical performance. With the addition of 1\u2005M methanol in 1\u2005M KOH, the optimized composition was able to electrochemically produce formate at 0.149\u2005mmol\u2009cm\n                    <jats:sup>\u22122<\/jats:sup>\n                    \u2009h\n                    <jats:sup>\u22121<\/jats:sup>\n                    with a Faradaic efficiency up to 95.1\u2009% at 0.6\u2005V versus Hg\/HgO within a 22\u2005h testing period. In 1\u2005M KOH solution without methanol, the supercapacitive performance was achieved at a specific capacitance of over 1500\u2005F\u2009g\n                    <jats:sup>\u22121<\/jats:sup>\n                    , and outstanding cycling stability with only approximately 20\u2009% decay after continuous 10000 charging\u2010discharging cycles. These results underscore that the prepared Ni\u2212Co alloy nanoparticles serve as multi\u2010functional electrodes for electrochemical energy conversion and storage, particularly in the MOR and supercapacitors applications.\n                  <\/jats:p>","DOI":"10.1002\/cssc.202401098","type":"journal-article","created":{"date-parts":[[2024,10,8]],"date-time":"2024-10-08T03:44:34Z","timestamp":1728359074000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":19,"title":["Enhanced Methanol Electrooxidation and Supercapacitive Performance via Compositional Engineering of Colloidal Ni\u2010Co Alloying Nanoparticles"],"prefix":"10.1002","volume":"18","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-1482-1972","authenticated-orcid":false,"given":"Junshan","family":"Li","sequence":"first","affiliation":[{"name":"Institute for Advanced Study Chengdu University  Chengdu 610106 China"},{"name":"State Key Laboratory of 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