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Copper (Cu)\u2010based electrocatalysts generally play the predominant role in this process. Yet recently, more and more non\u2010Cu materials have demonstrated the capability to convert CO<jats:sub>2<\/jats:sub> into C<jats:sub>2+<\/jats:sub>, which provides impressive production efficiency even exceeding those on Cu, and a wider variety of C<jats:sub>2+<\/jats:sub> compounds not achievable with Cu counterparts. This motivates us to organize the present review to make a timely and tutorial summary of recent progresses on developing non\u2010Cu based catalysts for CO<jats:sub>2<\/jats:sub>\u2010to\u2010C<jats:sub>2+<\/jats:sub>. We begin by elucidating the reaction pathways for C<jats:sub>2+<\/jats:sub> formation, with an emphasis on the unique C\u2212C coupling mechanisms in non\u2010Cu electrocatalysts. Subsequently, we summarize the typical C<jats:sub>2+<\/jats:sub>\u2010involved non\u2010Cu catalysts, including <jats:italic>ds<\/jats:italic>\u2010, <jats:italic>d<\/jats:italic>\u2010 and <jats:italic>p<\/jats:italic>\u2010block metals, as well as metal\u2010free materials, presenting the state\u2010of\u2010the\u2010art design strategies to enhance C<jats:sub>2+<\/jats:sub> efficiency. The system upgrading to promote C<jats:sub>2+<\/jats:sub> productivity on non\u2010Cu electrodes covering microbial electrosynthesis, electrolyte engineering, regulation of operational conditions, and synergistic co\u2010electrolysis, is highlighted as well. Our review concludes with an exploration of the challenges and future opportunities in this rapidly evolving field.<\/jats:p>","DOI":"10.1002\/cssc.202401173","type":"journal-article","created":{"date-parts":[[2024,7,10]],"date-time":"2024-07-10T03:26:01Z","timestamp":1720581961000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":16,"title":["Electrochemical CO<sub>2<\/sub> Reduction to Multicarbon Products on Non\u2010Copper Based Catalysts"],"prefix":"10.1002","volume":"18","author":[{"given":"Jiayi","family":"Huang","sequence":"first","affiliation":[{"name":"College of Chemistry and Materials Science Nanjing Normal University  Nanjing, Jiangsu 210023 P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qianwen","family":"Liu","sequence":"additional","affiliation":[{"name":"College of Chemistry and Materials Science Nanjing Normal University  Nanjing, Jiangsu 210023 P. R. 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