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This review emphasizes on innovative catalyst designs, including homogeneous and heterogenous catalysts tailored to low\u2010concentration reactive nitrogen species. Moreover it explores the integration of advanced separation and concentration techniques, such as electrosorption and dialysis, to overcome mass transport limitations and enable effective electrochemical valorization. This review also examines reactive separation strategies for post\u2010purification, focusing on the integration of recovery processes with catalysis in a direct manner. 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