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Developing efficient catalysts is the key to improve this carbon\u2010sulfur (C\u2212S) bond formation process. Herein, a novel catalyst, namely {Mo\n                    <jats:sub>2.89<\/jats:sub>\n                    W\n                    <jats:sub>0.11<\/jats:sub>\n                    S\n                    <jats:sub>4<\/jats:sub>\n                    }\n                    <jats:sub>n<\/jats:sub>\n                    , has been prepared by alloying engineering of its basal planes through an innovative synthetic methodology that makes use of isostructural building entities based on molybdenum and tungsten sulfide molecular complexes with M\n                    <jats:sub>3<\/jats:sub>\n                    S\n                    <jats:sub>4<\/jats:sub>\n                    (M=Mo, W) cluster cores. Besides excellent activity and reusability, {Mo\n                    <jats:sub>2.89<\/jats:sub>\n                    W\n                    <jats:sub>0.11<\/jats:sub>\n                    S\n                    <jats:sub>4<\/jats:sub>\n                    }\n                    <jats:sub>n<\/jats:sub>\n                    is of broad scope, enabling the conversion of structurally diverse thiols and primary as well as secondary alcohols into thioethers. A set of characterizations, in combination with catalytic results, reveal that the catalytic activity of {Mo\n                    <jats:sub>2.89<\/jats:sub>\n                    W\n                    <jats:sub>0.11<\/jats:sub>\n                    S\n                    <jats:sub>4<\/jats:sub>\n                    }\n                    <jats:sub>n<\/jats:sub>\n                    for this relevant transformation arises from the presence of multiple\u2010type active centers in the defective basal planes of this alloyed catalyst. More specifically, coordinatively unsaturated sulfurs and metal atoms with Lewis basic and Lewis acid properties, respectively, are proposed to be the active sites involved in the borrowing hydrogen mechanism.\n                  <\/jats:p>","DOI":"10.1002\/cssc.202500343","type":"journal-article","created":{"date-parts":[[2025,3,13]],"date-time":"2025-03-13T12:44:52Z","timestamp":1741869892000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":2,"title":["Alloying Engineering of Defective Molybdenum Sulfide Basal Planes for Enhanced Borrowing Hydrogen Activity in the Thioetherification of Alcohols"],"prefix":"10.1002","volume":"18","author":[{"given":"Miriam","family":"Rodenes","sequence":"first","affiliation":[{"name":"Instituto de Tecnolog\u00eda Qu\u00edmica Universitat Polit\u00e8cnica de Val\u00e8ncia-Consejo Superior de Investigaciones Cient\u00edficas (UPV-CSIC)  Av. de los Naranjos, s\/n 46022 Val\u00e8ncia Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Darija","family":"O\u0161tri\u0107","sequence":"additional","affiliation":[{"name":"Instituto de Tecnolog\u00eda Qu\u00edmica Universitat Polit\u00e8cnica de Val\u00e8ncia-Consejo Superior de Investigaciones Cient\u00edficas (UPV-CSIC)  Av. de los Naranjos, s\/n 46022 Val\u00e8ncia Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-9193-3874","authenticated-orcid":false,"given":"Santiago","family":"Mart\u00edn","sequence":"additional","affiliation":[{"name":"Instituto de Nanociencia y Materiales de Arag\u00f3n (INMA) Consejo Superior de Investigaciones Cient\u00edficas (CSIC)-Universidad de Zaragoza  50009 Zaragoza Spain"},{"name":"Departamento de Qu\u00edmica F\u00edsica, Facultad de Ciencias Universidad de Zaragoza  Zaragoza Spain"},{"name":"Laboratorio de Microscopias Avanzadas (LMA) Universidad de Zaragoza  50018 Zaragoza Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-2058-3103","authenticated-orcid":false,"given":"Patricia","family":"Concepci\u00f3n","sequence":"additional","affiliation":[{"name":"Instituto de Tecnolog\u00eda Qu\u00edmica Universitat Polit\u00e8cnica de Val\u00e8ncia-Consejo Superior de Investigaciones Cient\u00edficas (UPV-CSIC)  Av. de los Naranjos, s\/n 46022 Val\u00e8ncia Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-2232-3527","authenticated-orcid":false,"given":"Avelino","family":"Corma","sequence":"additional","affiliation":[{"name":"Instituto de Tecnolog\u00eda Qu\u00edmica Universitat Polit\u00e8cnica de Val\u00e8ncia-Consejo Superior de Investigaciones Cient\u00edficas (UPV-CSIC)  Av. de los Naranjos, s\/n 46022 Val\u00e8ncia Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-3721-9335","authenticated-orcid":false,"given":"Iv\u00e1n","family":"Sorribes","sequence":"additional","affiliation":[{"name":"Institute of Advanced Materials Universitat Jaume I  Av. 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