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We have summarized, compared, and critically evaluated state\u2010of\u2010the\u2010art experiments that help distinguish true piezocatalysis from sonocatalysis. We have highlighted the strengths and limitations of the current best practices for reliably confirming piezocatalytic activity. As an emerging field, we have outlined the present challenges in piezocatalytic and piezophotocatalytic organic synthesis (by C\u2013C, C\u2013N, and C\u2013O bonds coupling) and we have discussed the mechanistic role of piezoelectric effects in selectivity and bond activation. Finally, we offer our views on the future practical applications of using biomass resources. This goal has become a global research challenge in the search for a low\u2010carbon footprint for the future. Conventional techniques for converting biomass often struggle with inefficiency, low yield, and selectivity, as well as high energy demands. To overcome these issues, new methods that combine various processes, such as piezocatalysis and piezophotocatalysis, are becoming increasingly popular. We have focused our interest mainly on developments over the last 5 years.<\/jats:p>","DOI":"10.1002\/cssc.202501405","type":"journal-article","created":{"date-parts":[[2026,4,8]],"date-time":"2026-04-08T08:22:03Z","timestamp":1775636523000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":5,"title":["Synergistic Photocatalysis and Piezocatalysis in Organic Coupling: Mechanistic Insights, Perspectives, and Emerging Challenges"],"prefix":"10.1002","volume":"19","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-0391-8138","authenticated-orcid":false,"given":"Marta","family":"Paszkiewicz\u2010Gawron","sequence":"first","affiliation":[{"name":"Institute of Physical Chemistry Polish Academy of Sciences  Warsaw Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0009-2244-5047","authenticated-orcid":false,"given":"Pablo Martinez","family":"Marco","sequence":"additional","affiliation":[{"name":"Institute of Physical Chemistry Polish Academy of Sciences  Warsaw Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-8324-0119","authenticated-orcid":false,"given":"Fran\u00e7ois","family":"J\u00e9r\u00f4me","sequence":"additional","affiliation":[{"name":"Institut de Chimie des Milieux et Mat\u00e9riaux de Poitiers Universit\u00e9 de Poitiers\u2013CNRS  Poitiers France"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-4149-9720","authenticated-orcid":false,"given":"Emerson","family":"Coy","sequence":"additional","affiliation":[{"name":"NanoBioMedical Centre Adam Mickiewicz University  Poznan Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-1166-1982","authenticated-orcid":false,"given":"Ramon Fernando","family":"Colmenares\u2010Quintero","sequence":"additional","affiliation":[{"name":"Engineering Research Institute (In3) Universidad Cooperativa de Colombia  Medell\u00edn Colombia"},{"name":"Fundacion BERSTIC\u2014Science, Technology Innovation &amp; Culture Network  Medell\u00edn Colombia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3663-1122","authenticated-orcid":false,"given":"Dariusz","family":"\u0141omot","sequence":"additional","affiliation":[{"name":"Institute of Physical Chemistry Polish Academy of Sciences  Warsaw Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-3701-6340","authenticated-orcid":false,"given":"Juan Carlos","family":"Colmenares","sequence":"additional","affiliation":[{"name":"Institute of Physical Chemistry Polish Academy of Sciences  Warsaw Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2026,4,8]]},"reference":[{"key":"e_1_2_8_2_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.checat.2022.11.009"},{"key":"e_1_2_8_3_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.apcato.2024.206973"},{"key":"e_1_2_8_4_1","doi-asserted-by":"publisher","DOI":"10.1021\/acsami.4c03256"},{"key":"e_1_2_8_5_1","doi-asserted-by":"publisher","DOI":"10.1039\/D3EY00313B"},{"key":"e_1_2_8_6_1","doi-asserted-by":"crossref","unstructured":"H.Sudrajat H.\u2010Y.Hsu F.J\u00e9r\u00f4me andJ. 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