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This method relies on visible light\u2010induced oxidative dehydrogenative coupling between thiols and P(O)H compounds, utilizing lead\u2010free Cs\n                    <jats:sub>3<\/jats:sub>\n                    Bi\n                    <jats:sub>2<\/jats:sub>\n                    Br\n                    <jats:sub>9<\/jats:sub>\n                    perovskite as a heterogeneous photocatalyst with air serving as the oxidant. The reaction proceeds efficiently in 2\u2010methyl tetrahydrofuran (2\u2010MeTHF) under ambient temperature conditions, exhibits good tolerance towards a wide range of functional groups, and affords the target products in high yields. Furthermore, the photocatalyst can be readily recycled for at least 5 runs in gram\u2010scale synthesis without a significant loss of catalytic activity.\n                  <\/jats:p>","DOI":"10.1002\/cssc.202501607","type":"journal-article","created":{"date-parts":[[2025,9,27]],"date-time":"2025-09-27T13:55:29Z","timestamp":1758981329000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":4,"title":["Lead\u2010Free Cs\n                    <sub>3<\/sub>\n                    Bi\n                    <sub>2<\/sub>\n                    Br\n                    <sub>9<\/sub>\n                    Perovskite as Heterogeneous Photocatalyst for Oxidative Dehydrogenative Coupling of Thiols and P(O)H Compounds"],"prefix":"10.1002","volume":"18","author":[{"given":"Tong","family":"Yue","sequence":"first","affiliation":[{"name":"Hebei Key Laboratory of Organic Functional Molecules College of Chemistry and Materials Science Hebei Normal University  Shijiazhuang 050024 P. 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