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However, the conversion of lignin\u2010derived phenolic compounds to arenes typically requires high temperatures (above 300\u00b0C), which not only alters the catalyst structure and promotes side reactions but also increases energy consumption and potential safety risks. In this study, a green and environmentally friendly two\u2010step method for the low\u2010temperature conversion of phenol to benzene was proposed, achieving controllable product selectivity at low temperatures. The hydrogenation of phenol occurred efficiently at room temperature and achieved 100% conversion of cyclohexanol. Then, the dehydration and dehydrogenation of cyclohexanol was performed at a low temperature of 200\u00b0C, resulting in 90.1% selectivity of benzene. In addition, the catalyst showed good cycling stability, with the benzene selectivity remaining at 84.6% after four reaction cycles. Based on the effect of reaction time on product distribution, a proposed reaction pathway for cyclohexanol to benzene was discussed. Moreover, the comparison between this two\u2010step method and previously reported one\u2010step methods for phenol to benzene was carried out, highlighting the superiority of this work.<\/jats:p>","DOI":"10.1002\/cssc.70853","type":"journal-article","created":{"date-parts":[[2026,7,11]],"date-time":"2026-07-11T07:14:23Z","timestamp":1783754063000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["A Novel Two\u2010Step Conversion of Lignin\u2010Derived Phenol to Benzene Through Hydrogenation and Dehydrogenation"],"prefix":"10.1002","volume":"19","author":[{"ORCID":"https:\/\/orcid.org\/0000-0002-2904-5048","authenticated-orcid":false,"given":"Riyang","family":"Shu","sequence":"first","affiliation":[{"name":"Guangdong Provincial Key Laboratory of Functional Soft Condensed Matter School of Materials and Energy Guangdong University of Technology  Guangzhou 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