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However, the rational regulation of the lignin\u2010supported metal catalyst fabrication process to optimize their morphology and activity remains a challenge. Herein, we proposed a straightforward strategy to regulate the N content and species in the supports, thereby governing the nucleation behavior of Ru nanoparticles by varying the sintering temperature, for targeted enhancement of the catalytic performance of lignin\u2010supported Ru\u2010based catalysts. The sintering temperature of 700\u2009\u00b0C was conducive to reducing the escape of elemental N and maintaining a high percentage of pyridinic\u2010N species, which was beneficial to the adsorption and immobilization of Ru by the supports, resulting in the formation of Ru nanoparticles with a small size (1.93\u2009nm). In the catalytic transfer hydrogenation (CTH) of levulinic acid (LA) to \u03b3\u2010valerolactone (GVL) using isopropanol as the hydrogen donor, the obtained catalyst demonstrated nearly 100% LA conversion and GVL selectivity under mild conditions (120\u2009\u00b0C) with good reusability. This strategy achieves directional control over the structure of lignin\u2010supported metal catalysts through a simple method, providing guidance for the efficient synthesis of these catalysts.<\/jats:p>","DOI":"10.1002\/cssc.70936","type":"journal-article","created":{"date-parts":[[2026,7,31]],"date-time":"2026-07-31T12:20:51Z","timestamp":1785500451000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":1,"title":["Temperature\u2010Regulated N\u2010Involved Ru Nucleation on Lignin\u2010Derived Carbon for Enhanced Catalytic Transfer Hydrogenation of Levulinic Acid to \u03b3\u2010Valerolactone"],"prefix":"10.1002","volume":"19","author":[{"ORCID":"https:\/\/orcid.org\/0009-0008-2478-2875","authenticated-orcid":false,"given":"Tairan","family":"Pang","sequence":"first","affiliation":[{"name":"State Key Laboratory of Bio\u2010based Fiber Materials Tianjin Key Laboratory of Pulp and Paper College of Light Industry Science and Engineering Tianjin University of Science and Technology  Tianjin China"},{"name":"Robustnique Co. 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