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Herein, we report a low\u2010energy hydrothermal transformation strategy to fabricate two phase\u2010pure vanadium oxides (VO\n                    <jats:sub>2<\/jats:sub>\n                    and V\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>7<\/jats:sub>\n                    \u00b7H\n                    <jats:sub>2<\/jats:sub>\n                    O) without high temperature treatment. The tunnel\u2010structured VO\n                    <jats:sub>2<\/jats:sub>\n                    nanobelts with high oxygen vacancy defects can be obtained by the function of water\u2010soluble polymer sodium carboxymethyl cellulose (CMC), which plays a critical phase\u2010directing role by coordinating with released vanadium ions on the V\u2010MOF surface. As a cathode for aqueous zinc\u2010ion batteries (AZIBs), the VO\n                    <jats:sub>2<\/jats:sub>\n                    nanobelts deliver high specific capacities of 320.8\u2009mAh\u2009g\n                    <jats:sup>\u22121<\/jats:sup>\n                    at 0.1\u2009g\n                    <jats:sup>\u22121<\/jats:sup>\n                    and 242.2\u2009mAh\u2009g\n                    <jats:sup>\u22121<\/jats:sup>\n                    at 10\u2009A\u2009g\n                    <jats:sup>\u22121<\/jats:sup>\n                    , significantly outperforming the CMC\u2010free V\n                    <jats:sub>3<\/jats:sub>\n                    O\n                    <jats:sub>7<\/jats:sub>\n                    \u00b7H\n                    <jats:sub>2<\/jats:sub>\n                    O counterpart (309.5 and 162.3\u2009mAh\u2009g\n                    <jats:sup>\u22121<\/jats:sup>\n                    ). Moreover, VO\n                    <jats:sub>2<\/jats:sub>\n                    exhibits a high\u2010capacity retention of 73.6% after 1400 cycles at 10\u2009A g\n                    <jats:sup>\u22121<\/jats:sup>\n                    . The enhanced electrochemical behavior arises from the synergistic effects of the tunnel structure, uniform nanobelt morphology, and abundant oxygen vacancies, which facilitate Zn\n                    <jats:sup>2+<\/jats:sup>\n                    diffusion and electronic conduction. This work not only provides a high\u2010performance VO\n                    <jats:sub>2<\/jats:sub>\n                    cathode for AZIBs but also establishes a general, low\u2010cost, and scalable hydrothermal route for phase\u2010engineered MOF\u2010derived metal oxides.\n                  <\/jats:p>","DOI":"10.1002\/cssc.71013","type":"journal-article","created":{"date-parts":[[2026,8,27]],"date-time":"2026-08-27T06:17:13Z","timestamp":1787811433000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Carboxymethyl Cellulose\u2010Induced Phase Transformation of Metal\u2010Organic Framework\u2010Derived Vanadium Oxides for High\u2010Rate and High\u2010Capacity Zinc Storage"],"prefix":"10.1002","volume":"19","author":[{"given":"Wei","family":"Xia","sequence":"first","affiliation":[{"name":"College of Electrical Engineering and New Energy China Three Gorges University  Yichang Hubei P. R. China"},{"name":"Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials College of Materials and Chemical Engineering China Three Gorges University  Yichang Hubei P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yaxuan","family":"Wang","sequence":"additional","affiliation":[{"name":"Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials College of Materials and Chemical Engineering China Three Gorges University  Yichang Hubei P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Zhizhi","family":"Xu","sequence":"additional","affiliation":[{"name":"Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials College of Materials and Chemical Engineering China Three Gorges University  Yichang Hubei P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Yongkang","family":"Ye","sequence":"additional","affiliation":[{"name":"Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials College of Materials and Chemical Engineering China Three Gorges University  Yichang Hubei P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xi\u2010Wen","family":"Chang","sequence":"additional","affiliation":[{"name":"College of Electrical Engineering and New Energy China Three Gorges University  Yichang Hubei P. R. China"},{"name":"Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials College of Materials and Chemical Engineering China Three Gorges University  Yichang Hubei P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ya\u2010Meng","family":"Yin","sequence":"additional","affiliation":[{"name":"Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials College of Materials and Chemical Engineering China Three Gorges University  Yichang Hubei P. R. China"},{"name":"Hubei Three Gorges Laboratory  Yichang Hubei P. R. China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0009-0003-0340-1491","authenticated-orcid":false,"given":"Cai\u2010Hong","family":"Yang","sequence":"additional","affiliation":[{"name":"Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials College of Materials and Chemical Engineering China Three Gorges University  Yichang Hubei P. R. China"},{"name":"Hubei Three Gorges Laboratory  Yichang Hubei P. R. 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