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Extraction procedures applied to the analysis of their formulations are still limited to a few methodologies, despite the increasing numbers of confiscations of AASs. In this sense, the aims of this work were to evaluate the extraction of active ingredients from formulations of anabolic agents using solid\u2010liquid or liquid\u2010iquid, ultrasonic bath, ultrasonicprobe, and microwave\u2010assisted extraction. The results indicated that the extraction procedures influenced the detected concentration of AASs, as the use of ultrasonic probe and microwave irradiation increased the overall extraction of anabolic agents compared with solid\u2010liquid, liquid\u2010liquid, and ultrasonic bath. Regarding oxymetholone, for instance, the microwave\u2010assisted extraction and ultrasonic probe extracted, respectively, 37.46 \u00b1 1.36 and 35.69 \u00b1 0.98 mg\/tablet, while solid\u2010liquid extracted 29.63 \u00b1 0.40 mg\/tablet of the activeingredient. Therefore, alternative methods such as microwave\u2010assisted extraction or theultrasonic probe could be used for the analysis of formulations of AASs assisting with the identification of illicit and toxic components.<\/jats:p>","DOI":"10.1002\/dta.2877","type":"journal-article","created":{"date-parts":[[2020,6,14]],"date-time":"2020-06-14T22:15:49Z","timestamp":1592172949000},"page":"1264-1273","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":6,"title":["Analytical approaches applied to the analysis of apprehended formulations of anabolic androgenic steroids"],"prefix":"10.1002","volume":"12","author":[{"given":"Lucas M.","family":"Berneira","sequence":"first","affiliation":[{"name":"Center of Chemical, Pharmaceutical and Food Sciences, Lipidomic and Bio\u2010Organic Laboratory, Bioforensic Research Group Federal University of Pelotas  Pelotas RS Brazil"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Caroline 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