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The reaction product is isolated in a dimeric form with a planar Zn<jats:sub>2<\/jats:sub>(\u00b5\u2010O)<jats:sub>2<\/jats:sub>\u2010motif keeping the two monomers together. This compound can serve as a model for reactive intermediates in the catalytic alkylation of ketones with diorganozinc reagents. Hydrolysis of this binuclear zinc compound leads to isolation of the C\u2010alkylated product in 89\u2009% yield. A reaction pathway is proposed in which BM<jats:sup>diPh<\/jats:sup>IK initially coordinates to diethylzinc as a bidentate bis(nitrogen) ligand. This is followed by the homolytic cleavage of the Zn\u2013Et bond and in\u2010cage recombination of the Et\u2010radical and the Zn\u2010coordinated ligand\u2010centered radical, which is mainly localized on the carbonyl moiety of the ligand.<\/jats:p>","DOI":"10.1002\/ejic.201701363","type":"journal-article","created":{"date-parts":[[2018,2,12]],"date-time":"2018-02-12T08:36:46Z","timestamp":1518424606000},"page":"1167-1175","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":3,"title":["1,2\u2010Addition of Diethylzinc to a Bis(Imidazolyl)ketone Ligand"],"prefix":"10.1002","volume":"2018","author":[{"given":"Emma","family":"Folkertsma","sequence":"first","affiliation":[{"name":"Organic Chemistry &amp; Catalysis Debye Institute for Nanomaterials Science Utrecht University  Universiteitsweg 99 3584 CG Utrecht The Netherlands"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Sanne H.","family":"Benthem","sequence":"additional","affiliation":[{"name":"Organic Chemistry &amp; Catalysis Debye Institute for Nanomaterials Science Utrecht University  Universiteitsweg 99 3584 CG Utrecht The Netherlands"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Johann T. 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