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Imidazole was confirmed not only as a co\u2013ion for the separation but also as an online complexing reagent for mercury species. The optimum conditions for separation were achieved by using methanol solvent containing 0.15\u2005<jats:sc>M<\/jats:sc> acetic acid and 15\u2009m<jats:sc>M<\/jats:sc> imidazole as electrolyte. 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