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The prepared monoliths were characterized by FTIR spectrometry, mercury intrusion porosimeter and SEM, while their performance was evaluated by CEC for the separation of various types of compounds including alkyl benzenes, polycyclic aromatic hydrocarbons, nonsteroidal anti\u2010inflammatory drugs, anilines, and nitrophenol isomers. The column\u2010to\u2010column and batch\u2010to\u2010batch reproducibility for the prepared monoliths in terms of the RSD of EOF flow velocity, retention factor, and the minimum plate height of naphthalene ranged from 3.4 to 12.4%. The fabricated monoliths gave excellent performance for the separation of the test neutral compounds with the theoretical plates of 170\u2009000\u2013232\u2009000 plates <jats:italic>per<\/jats:italic> meter for thiourea, and 77\u2009400\u2013112\u2009300 plates <jats:italic>per<\/jats:italic> meter for naphthalene. The proposed strong inorganic acid\u2010initiated methacrylate polymerization strategy is a promising alternative for fabricating organic polymer\u2010based monoliths.<\/jats:p>","DOI":"10.1002\/elps.200900756","type":"journal-article","created":{"date-parts":[[2010,4,21]],"date-time":"2010-04-21T13:09:57Z","timestamp":1271855397000},"page":"1666-1673","source":"Crossref","is-referenced-by-count":11,"title":["A strong inorganic acid\u2010initiated methacrylate polymerization strategy for room temperature preparation of monolithic columns for capillary 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