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A sensitization of MF was provoked by UV irradiation of analytes in a home\u2010made photoreactor that served as interface between the LC column and MF spectrometer. This method is applied to determination of THM, ethyl mercury, and thiosalicylic acid in samples of pharmaceutical industry effluents, and waters of La Carolina and J\u00e1chal rivers situated in the center\u2010west side of San Luis city and in the east of San Juan city (Middle West, Argentine) where the effluents are dumped. 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