{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,9,18]],"date-time":"2026-09-18T07:04:27Z","timestamp":1789715067157,"version":"4.0.1"},"reference-count":29,"publisher":"Wiley","license":[{"start":{"date-parts":[[2026,9,17]],"date-time":"2026-09-17T00:00:00Z","timestamp":1789603200000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"},{"start":{"date-parts":[[2026,9,17]],"date-time":"2026-09-17T00:00:00Z","timestamp":1789603200000},"content-version":"tdm","delay-in-days":0,"URL":"http:\/\/doi.wiley.com\/10.1002\/tdm_license_1.1"}],"content-domain":{"domain":["analyticalsciencejournals.onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["Electrophoresis"],"abstract":"<jats:title>ABSTRACT<\/jats:title>\n                  <jats:p>\n                    The increasing consumption of plant\u2010based beverages (PBBs), driven by ethical and health\u2010related reasons, highlights the need for robust analytical methods assessing their chemical safety. Among these products, hazelnut\u2010based beverages are of particular interest in Italy, where hazelnut production is economically relevant. A rapid one\u2010step extraction procedure was developed for the multiresidue determination of selected chiral and achiral pesticides in PBBs by ultra\u2010high\u2010performance liquid chromatography\u2013high resolution mass spectrometry (UHPLC\u2013HRMS). The method combines matrix precipitation and analyte extraction in a single step, providing a simple and efficient workflow. Validation, carried out in hazelnut beverage, included recovery, precision, linearity, decision limit (CC\u03b1), and detection capability (CC\u03b2) evaluation. As no European Union maximum residue levels (MRLs) are available for PBBs, provisional MRLs for hazelnut milk were derived from raw hazelnut MRLs using a recipe\u2010based processing factor, according to Regulation (EC) No 396\/2005. The method achieved recoveries of 60%\u201390%, intra\u2010 and inter\u2010day precision generally below 20%, CC\u03b1 values of 0.001\u20130.016\u00a0\u00b5g\u00a0L\n                    <jats:sup>\u22121<\/jats:sup>\n                    , CC\u03b2 values of 0.002\u20130.027\u00a0\u00b5g\u00a0L\n                    <jats:sup>\u22121<\/jats:sup>\n                    , and good linearity for most analytes (\n                    <jats:italic>R<\/jats:italic>\n                    <jats:sup>2<\/jats:sup>\n                    \u00a0&gt;\u00a00.99). The proposed procedure is suitable for pesticide residue analysis in PBBs, such as hazelnut\u2010based beverages, and represents a valuable approach for monitoring emerging food matrices, for which residue data and regulatory limits are still lacking.\n                  <\/jats:p>","DOI":"10.1002\/elps.70154","type":"journal-article","created":{"date-parts":[[2026,9,18]],"date-time":"2026-09-18T06:47:53Z","timestamp":1789714073000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["A Streamlined Single\u2010Step Salting\u2010Out Approach for Chiral and Achiral Pesticide Analysis in Hazelnut\u2010Based Beverages"],"prefix":"10.1002","author":[{"given":"Giulia","family":"Bertini","sequence":"first","affiliation":[{"name":"Department of Chemistry Sapienza University of Rome  Rome Italy"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Davide","family":"Vona","sequence":"additional","affiliation":[{"name":"Department of Chemistry Sapienza University of Rome  Rome Italy"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Nina","family":"Felli","sequence":"additional","affiliation":[{"name":"Department of Chemistry Sapienza University of Rome  Rome Italy"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Lorenzo","family":"Antonelli","sequence":"additional","affiliation":[{"name":"Department of Chemistry Sapienza University of Rome  Rome Italy"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Salvatore","family":"Fanali","sequence":"additional","affiliation":[{"name":"Institute of Physical and Analytical Chemistry School of Exact and Natural Sciences Tbilisi State University  Tbilisi Georgia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Chiara","family":"Fanali","sequence":"additional","affiliation":[{"name":"Department of Science and Technology for Sustainable Development and One Health Universit\u00e0 Campus Bio\u2010Medico Di Roma  Rome Italy"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Stefania","family":"Carpino","sequence":"additional","affiliation":[{"name":"Department of Central Inspectorate for Fraud Repression and Quality Protection of the Agri\u2010Food Products and Foodstuffs Ministry of Agriculture Food Sovereignty and Forests (ICQRF\u2010MASAF)  Rome Italy"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Vincenzo","family":"Di Martino","sequence":"additional","affiliation":[{"name":"Department of Central Inspectorate for Fraud Repression and Quality Protection of the Agri\u2010Food Products and Foodstuffs Ministry of Agriculture Food Sovereignty and Forests (ICQRF\u2010MASAF)  Rome Italy"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Chiara","family":"Cavaliere","sequence":"additional","affiliation":[{"name":"Department of Chemistry Sapienza University of Rome  Rome Italy"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-9541-3857","authenticated-orcid":false,"given":"Alessandra","family":"Gentili","sequence":"additional","affiliation":[{"name":"Department of Chemistry Sapienza University of Rome  Rome Italy"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2026,9,17]]},"reference":[{"key":"e_1_2_9_2_1","doi-asserted-by":"publisher","DOI":"10.1002\/fsn3.71590"},{"key":"e_1_2_9_3_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.foodchem.2026.149386"},{"key":"e_1_2_9_4_1","doi-asserted-by":"publisher","DOI":"10.1002\/elps.201200079"},{"key":"e_1_2_9_5_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.lwt.2023.115688"},{"key":"e_1_2_9_6_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.ifset.2017.05.002"},{"key":"e_1_2_9_7_1","doi-asserted-by":"publisher","DOI":"10.3390\/nu13030842"},{"key":"e_1_2_9_8_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.foohum.2024.100301"},{"key":"e_1_2_9_9_1","doi-asserted-by":"publisher","DOI":"10.3390\/foods9050682"},{"key":"e_1_2_9_10_1","doi-asserted-by":"publisher","DOI":"10.3390\/nu15153415"},{"key":"e_1_2_9_11_1","doi-asserted-by":"publisher","DOI":"10.1080\/10942912.2022.2134417"},{"key":"e_1_2_9_12_1","doi-asserted-by":"publisher","DOI":"10.1111\/1541\u20104337.70460"},{"key":"e_1_2_9_13_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.fochx.2026.103528"},{"key":"e_1_2_9_14_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.foodcont.2024.111005"},{"key":"e_1_2_9_15_1","unstructured":"European Commission Commission Regulation (EU) 2023\/915 of 25 April 2023 on maximum levels for certain contaminants in food and repealing Regulation (EC) No 1881\/2006 Off. 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