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Recently, encouraging progress has been made in tuning the structure and composition of HEAs used in electrolyzers and fuel cells. However, the understanding on the synthetic methods and the structure\u2010property\u2010performance relationship of well\u2010defined HEAs nanostructures is still inadequate. To gain insight into the future research directions on HEAs for electrocatalysis, in this paper, the synthetic methods commonly used to obtain well\u2010defined HEAs nanostructures (0D nanoparticles, 1D nanowires, 2D nanosheets\/nanoplates, 3D nanoporous structures, and other three\u2010dimensional morphologies) are first summarized. Then, the authors discuss the application of well\u2010defined HEAs nanostructures in several typical electrocatalytic reactions, including hydrogen evolution reaction, oxygen evolution reaction, oxygen reduction reaction, alcohol oxidation reaction, carbon dioxide reduction reaction, nitrogen reduction reaction, and formic acid oxidation reaction. Finally, a practical perspective on the future research directions on well\u2010defined HEAs nanostructured electrocatalysts is provided.<\/jats:p>","DOI":"10.1002\/exp.20230036","type":"journal-article","created":{"date-parts":[[2024,7,2]],"date-time":"2024-07-02T12:06:07Z","timestamp":1719921967000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":71,"title":["Well\u2010defined nanostructures of high entropy alloys for electrocatalysis"],"prefix":"10.1002","volume":"5","author":[{"given":"Jie","family":"Chen","sequence":"first","affiliation":[{"name":"School of Chemical Engineering and Technology Xi'an Jiaotong University  Xi'an China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Liping","family":"Ren","sequence":"additional","affiliation":[{"name":"School of Chemical Engineering and Technology Xi'an Jiaotong University  Xi'an China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Xin","family":"Chen","sequence":"additional","affiliation":[{"name":"School of Chemical Engineering and Technology Xi'an Jiaotong University  Xi'an China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Qi","family":"Wang","sequence":"additional","affiliation":[{"name":"School of Chemical Engineering and Technology Xi'an Jiaotong University  Xi'an China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Chunying","family":"Chen","sequence":"additional","affiliation":[{"name":"School of Chemical Engineering and Technology Xi'an Jiaotong University  Xi'an China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Jinpeng","family":"Fan","sequence":"additional","affiliation":[{"name":"School of Chemical Engineering and Technology Xi'an Jiaotong University  Xi'an China"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Shuai","family":"Wang","sequence":"additional","affiliation":[{"name":"China Coal Energy Research Institute Co., Ltd.  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