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Using knowledge of OSC morphology, an insertion strategy involved adding a suitable quantity of guest acceptor (Y6\u2010O) to the PM6 donor polymer and BTP\u20102F\u2010ThCl host small molecule acceptor system. Y6\u2010O leads to tighter \u03c0\u2013\u03c0 packing, reduced domain size, and improved domain purity, resulting in favorable morphology for charge generation and transfer in devices and an improved power conversion efficiency (PCE) from 17.1% to 18.1%. Moreover, terpolymer organic photovoltaic films were applied to wastewater treatment, gaining ions Sb(III) and Sb(V) removals of 100% in 15\u00a0min, and guaiacol photodegradations of 90% in 1\u00a0h. 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