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From the experimental processes and the characterization of the crystals it was concluded that aging and precipitation kinetics are critical for the purity of the product and its crystallographic characteristics. The authentication details are presented along with the results from infrared spectroscopy, X\u2010ray powder diffraction, Raman spectroscopy, transmission and scanning electron photographs,  and chemical analysis. Analytical data for several calcium phosphates were collected from the literature, extensively reviewed, and the results were grouped and presented in tables to provide comparison with the data obtained here. \u00a9 2002 Wiley Periodicals, Inc. 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