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The effects of the thickness of the \u03b3\u2010MPS layer on the shear bonding strength between Ti and SPU were investigated. Ti disks were immersed in various concentrations of \u03b3\u2010MPS solutions for several immersion times. The depth profiles of elements and the thickness of the \u03b3\u2010MPS layer were determined by glow discharge optical emission spectroscopy and ellipsometry, respectively. The bonding stress at the Ti\/\u03b3\u2010MPS\/SPU interface was evaluated with a shear bonding test. Furthermore, the fractured surface of a Ti\u2010SPU composite was observed by optical microscopy and characterized using X\u2010ray photoelectron spectroscopy. Consequently, the thickness of the \u03b3\u2010MPS layer was controlled by the concentration of the \u03b3\u2010MPS solution and immersion time. The shear bonding stress at the interface increased with the increase of the thickness of the \u03b3\u2010MPS layer. Therefore, the control of the thickness of the \u03b3\u2010MPS layer is significant to increase the shear bonding stress at the Ti\/\u03b3\u2010MPS\/SPU interface. These results are significant to create composites for artificial organs consisting of other metals and polymers. \u00a9 2007 Wiley Periodicals, Inc. 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