{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2023,10,24]],"date-time":"2023-10-24T05:40:33Z","timestamp":1698126033936},"reference-count":10,"publisher":"Wiley","issue":"4","license":[{"start":{"date-parts":[[2005,10,20]],"date-time":"2005-10-20T00:00:00Z","timestamp":1129766400000},"content-version":"vor","delay-in-days":5041,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["Clinical Laboratory Analysis"],"published-print":{"date-parts":[[1992,1]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>A simple and sensitive procedure for total mercury in whole blood and urine using inductively coupled plasma\u2010mass spectrometry (ICP\u2010MS) is described. Specimens are prepared by precipitation\u2010extraction with 50% v\/v hydrochloric acid containing EDTA and cysteine, centrifuged, and filtered through fritended screening column; the filtrates are directly analyzed by ICP\u2010MS. The method is linear between 2 and 200 \u03bcg\/L in the specimen with an absolute sensitivity of 0.2 \u03bcg\/L in the final supernatant. The assay variability at various concentrations (\u03bcg\/L) of mercury are as follows: intra\u2010assay whole blood (n = 20)\u20144.6 \u00b1 0.6(c.v. 12.3%), 18.3 \u00b1 1.1(c.v.6.1%), 56.4 \u00b1 2.8(c.v.5.0%); inter\u2010assay whole blood (n = 15)\u20145.7 \u00b1 1.0(c.v.16.8%), 19.7 \u00b1 2.7(c.v. 13.5%), and 50.1 \u00b1 6.9(c.v.13.7%); urine (n = 20)\u20149.3 \u00b1 1.2 (c.v. 12.9%), 29.6 \u00b1 2.2 (c.v. 7.4%). Recovery of organic and inorganic mercury from blood samples ranges from 91.6% to 110.2%. The method is suitable for analysis of total mercury, both organic and inorganic, in whole blood and urine. \u00a9 1992 Wiley\u2010Liss, Inc.<\/jats:p>","DOI":"10.1002\/jcla.1860060405","type":"journal-article","created":{"date-parts":[[2007,3,5]],"date-time":"2007-03-05T20:22:35Z","timestamp":1173126155000},"page":"190-193","source":"Crossref","is-referenced-by-count":8,"title":["A simple ICP\u2010MS procedure for the determination of total mercury in whole blood and urine"],"prefix":"10.1002","volume":"6","author":[{"given":"Ramaswami","family":"Kalamegham","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"K. Owen","family":"Ash","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2005,10,20]]},"reference":[{"key":"e_1_2_1_2_2","volume-title":"Inorganic Mercury, Environmental Health Criteria 118","author":"WHO","year":"1991"},{"key":"e_1_2_1_3_2","volume-title":"Methyl Mercury, Environment Health Criteria 101","author":"WHO","year":"1990"},{"key":"e_1_2_1_4_2","first-page":"94","volume-title":"Threshold limit values for chemical substances and physical agents in the workroom environment with intended changes for 1976","author":"American Conference of Governmental Industrial Hygienists","year":"1976"},{"key":"e_1_2_1_5_2","first-page":"553","volume-title":"Quantitative Trace Analysis of Biological Materials","author":"Boiteau HL","year":"1988"},{"key":"e_1_2_1_6_2","first-page":"36","article-title":"ICP\u2010MS: An alternative method for the USEPA contract laboratory program","volume":"21","author":"Pruszkowski E","year":"1989","journal-title":"Am Lab"},{"key":"e_1_2_1_7_2","doi-asserted-by":"publisher","DOI":"10.1021\/ac00126a061"},{"key":"e_1_2_1_8_2","doi-asserted-by":"publisher","DOI":"10.1366\/0003702904086830"},{"key":"e_1_2_1_9_2","doi-asserted-by":"publisher","DOI":"10.1021\/ac00174a012"},{"key":"e_1_2_1_10_2","doi-asserted-by":"publisher","DOI":"10.1021\/ac00292a003"},{"key":"e_1_2_1_11_2","first-page":"266","volume-title":"Official Methods of Analysis of the AOAC","author":"AOAC","year":"1990"}],"container-title":["Journal of Clinical Laboratory Analysis"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/api.wiley.com\/onlinelibrary\/tdm\/v1\/articles\/10.1002%2Fjcla.1860060405","content-type":"unspecified","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/onlinelibrary.wiley.com\/doi\/pdf\/10.1002\/jcla.1860060405","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2023,10,23]],"date-time":"2023-10-23T17:28:55Z","timestamp":1698082135000},"score":1,"resource":{"primary":{"URL":"https:\/\/onlinelibrary.wiley.com\/doi\/10.1002\/jcla.1860060405"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[1992,1]]},"references-count":10,"journal-issue":{"issue":"4","published-print":{"date-parts":[[1992,1]]}},"alternative-id":["10.1002\/jcla.1860060405"],"URL":"https:\/\/doi.org\/10.1002\/jcla.1860060405","archive":["Portico"],"relation":{},"ISSN":["0887-8013","1098-2825"],"issn-type":[{"value":"0887-8013","type":"print"},{"value":"1098-2825","type":"electronic"}],"subject":[],"published":{"date-parts":[[1992,1]]}}}