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This work valorized a waste by\u2010product from olive (<jats:italic>Olea europaea<\/jats:italic> L.) milling into functional hydrochar (HC). The HC was then transformed into iron oxide\u2013encapsulated carbon with three different iron loading rates (10, 25, and 50% w\/w of iron chloride hexahydrate added to the olive mill waste feedstock). The HC and the three iron oxide\u2013encapsulated carbon materials were then tested in a pot trial using a 3% w\/w application rate as a means to immobilize As in a mining\u2010contaminated soil (2,580\u00a0\u00b1\u00a0110\u00a0mg kg<jats:sup>\u22121<\/jats:sup> As). After a 45\u2010d incubation period, the effect of adding the amendments on As mobility and bioaccessibility compared with an untreated control was measured using a sequential extraction procedure and in vitro bioaccessibility, respectively. All four treatments resulted in a decrease in mobility and in vitro bioaccessibility as compared with the control. Specifically, As in the mobile phases was up to 35% less than the in control, whereas bioaccessibility was 21.8% in the control and ranged from 17.5 to 12.3% in the treatments. The efficiency of amendments to immobilize As increased with the iron content of the developed materials. This work positions HCs and iron oxide\u2013encapsulated carbon materials produced from olive mill waste as promising options to immobilize As in situ.<\/jats:p>","DOI":"10.1002\/jeq2.20439","type":"journal-article","created":{"date-parts":[[2022,11,25]],"date-time":"2022-11-25T19:39:10Z","timestamp":1669405150000},"page":"161-172","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":5,"title":["Arsenic immobilization in soil affected by mining waste using waste\u2010derived functional hydrochar and iron\u2010encapsulated materials"],"prefix":"10.1002","volume":"52","author":[{"given":"Muhammad","family":"Haris","sequence":"first","affiliation":[{"name":"School of Engineering RMIT Univ.  Melbourne VIC 3000 Australia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Pacian","family":"Netherway","sequence":"additional","affiliation":[{"name":"Environment Protection Authority Victoria, EPA Science  Terrace 4 Ernest Jones Dr. Macleod VIC 3085 Australia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Nicky","family":"Eshtiaghi","sequence":"additional","affiliation":[{"name":"School of Engineering RMIT Univ.  Melbourne VIC 3000 Australia"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8169-4099","authenticated-orcid":false,"given":"Jorge","family":"Paz\u2010Ferreiro","sequence":"additional","affiliation":[{"name":"School of Engineering RMIT Univ.  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