{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,1,8]],"date-time":"2026-01-08T05:25:09Z","timestamp":1767849909277,"version":"3.49.0"},"reference-count":31,"publisher":"Wiley","issue":"3","license":[{"start":{"date-parts":[[2020,2,8]],"date-time":"2020-02-08T00:00:00Z","timestamp":1581120000000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"name":"Research Project of Qingdao Customs District","award":["QK201916"],"award-info":[{"award-number":["QK201916"]}]},{"name":"Public Science and Technology Project of Qingdao","award":["18-6-1-107-nsh"],"award-info":[{"award-number":["18-6-1-107-nsh"]}]}],"content-domain":{"domain":["analyticalsciencejournals.onlinelibrary.wiley.com"],"crossmark-restriction":true},"short-container-title":["J Mass Spectrom"],"published-print":{"date-parts":[[2020,3]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>A multiclass and multiresidue method for screening veterinary drugs and pesticides in infant formula was developed and validated using ultrahigh\u2010performance liquid chromatography coupled to Quadrupole\u2010Orbitrap high\u2010resolution mass spectrometry (UHPLC\u2010HRMS). A total of 49 veterinary drugs and pesticides investigated belong to 11 classes including antivirals, anticoccidials, macrolides, pyrethroids, insecticides, sulfonamides, beta\u2010agonists, sedatives, thyreostats, nonsteroidal anti\u2010inflammatory drugs, and other pharmacologically active substances. A generic sample preparation and highly selective acquisition mode of parallel reaction monitoring (PRM) were deliberately incorporated to perform efficient screening analysis. As a result, the screening target concentrations of the analytes varied from 1 to 500 \u03bcg\/kg with \u22645% of false compliant rate as specified in Decision 2002\/657\/EC for screening analysis. The average recoveries ranged from 40.7 to 124.9% as well as the relative standard deviations from 4.2 to 26.6%, respectively. The matrix effects and interferences were effectively controlled by integrated application of dispersive solid phase extraction, PRM scan mode, and matrix\u2010matched standard calibration. The proposed method will be helpful to provide applicable strategy for screening residues in infant formula with surveillance purpose.<\/jats:p>","DOI":"10.1002\/jms.4497","type":"journal-article","created":{"date-parts":[[2020,1,9]],"date-time":"2020-01-09T19:34:15Z","timestamp":1578598455000},"update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":9,"title":["Multiclass and multiresidue screening of veterinary drugs and pesticides in infant formula using Quadrupole\u2010Orbitrap MS with PRM scan mode"],"prefix":"10.1002","volume":"55","author":[{"ORCID":"https:\/\/orcid.org\/0000-0001-9462-1075","authenticated-orcid":false,"given":"Lu\u2010Qi","family":"Zhang","sequence":"first","affiliation":[{"name":"Technology Center of Qingdao Customs District  Qingdao PR China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Xiao\u2010Mei","family":"Zhang","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs District  Qingdao PR China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"ORCID":"https:\/\/orcid.org\/0000-0001-8328-6208","authenticated-orcid":false,"given":"Hong\u2010Wei","family":"Zhang","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs District  Qingdao PR China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Hui","family":"Wang","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs District  Qingdao PR China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Hui","family":"Xu","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs District  Qingdao PR China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Feng\u2010Mei","family":"Wang","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs District  Qingdao PR China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Chao","family":"Lin","sequence":"additional","affiliation":[{"name":"Technology Center of Qingdao Customs District  Qingdao PR China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Jing","family":"Xiao","sequence":"additional","affiliation":[{"name":"China National Center for Food Safety Risk Assessment  Beijing PR China"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Wen\u2010Yuan","family":"Xu","sequence":"additional","affiliation":[{"name":"Comprehensive Technical Service Center of Linyi Customs  Linyi PR China"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2020,2,8]]},"reference":[{"key":"e_1_2_7_2_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.foodchem.2012.04.076"},{"key":"e_1_2_7_3_1","doi-asserted-by":"publisher","DOI":"10.1007\/s12161-013-9683-8"},{"key":"e_1_2_7_4_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jchromb.2015.08.005"},{"key":"e_1_2_7_5_1","doi-asserted-by":"publisher","DOI":"10.1002\/jms.3834"},{"key":"e_1_2_7_6_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.aca.2017.01.046"},{"key":"e_1_2_7_7_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.jpba.2014.09.005"},{"key":"e_1_2_7_8_1","unstructured":"Bulletin No.235 Ministry of Agriculture PR China. 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