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They possess a wealth of secondary metabolites with potential antidiabetic activity. The present study investigated this by identifying volatile constituents associated with\n                      <jats:italic>in vitro<\/jats:italic>\n                      inhibition of\n                      <jats:italic>\u03b1<\/jats:italic>\n                      \u2010glucosidase derived from bio\u2010guided hexane fractions of\n                      <jats:italic>A. potatorum<\/jats:italic>\n                      Zucc. leaves. The process involved extraction followed by silica\u2010gel column chromatography, along with bioautography and ultraviolet\u2010visible (UV\u2010visible) assays, using acarbose as the positive control. The two most promising bio\u2010guided fractions were characterized using Attenuated Total Reflection Fourier\u2010Transform Infrared (ATR\u2010FTIR) spectroscopy, phytochemical screening, and gas chromatography\u2013mass spectrometry (GC\u2013MS). Their\n                      <jats:italic>in silico<\/jats:italic>\n                      properties were evaluated through absorption, distribution, metabolism, and excretion (ADME) analysis and molecular docking.\n                    <\/jats:p>\n                  <\/jats:sec>\n                  <jats:sec>\n                    <jats:title>RESULTS<\/jats:title>\n                    <jats:p>\n                      Two fractions exhibited higher\n                      <jats:italic>\u03b1<\/jats:italic>\n                      \u2010glucosidase inhibitory activity with inhibitory concentration (IC\n                      <jats:sub>50<\/jats:sub>\n                      ) values significantly lower than that of acarbose; however, none of the fractions achieved 50% inhibition of\n                      <jats:italic>\u03b1<\/jats:italic>\n                      \u2010amylase. The inhibitory activity may be attributed to unsaturated metabolites with terpenoid\u2010like structures. Twenty\u2010three volatile organic compounds (VOCs) were identified in these two fractions by GC\u2013MS. Among the compounds potentially associated with inhibitory activity of\n                      <jats:italic>\u03b1<\/jats:italic>\n                      \u2010glucosidase are dodecan\u20101\u2010ol, 2,4\u2010di\u2010\n                      <jats:italic>tert<\/jats:italic>\n                      \u2010butylphenol, tetradecane, and benzophenone. The\n                      <jats:italic>in silico<\/jats:italic>\n                      analysis indicated that the VOCs that were identified were not expected to accumulate in the human body, and molecular docking suggested that the inhibitory effects of the identified ligands may be mediated by hydrophobic interactions and hydrogen bonding.\n                    <\/jats:p>\n                  <\/jats:sec>\n                  <jats:sec>\n                    <jats:title>CONCLUSION<\/jats:title>\n                    <jats:p>\n                      This research supports the revalorization of agave byproducts as a viable source of secondary metabolites capable of influencing glucose absorption by\n                      <jats:italic>\u03b1<\/jats:italic>\n                      \u2010glucosidase, which is a therapeutic target for addressing type 2 diabetes mellitus, the second leading cause of death worldwide. \u00a9 2026 Society of Chemical Industry.\n                    <\/jats:p>\n                  <\/jats:sec>","DOI":"10.1002\/jsfa.70803","type":"journal-article","created":{"date-parts":[[2026,6,16]],"date-time":"2026-06-16T04:11:26Z","timestamp":1781583086000},"page":"7757-7774","update-policy":"https:\/\/doi.org\/10.1002\/crossmark_policy","source":"Crossref","is-referenced-by-count":0,"title":["Valorization of\n                    <i>Agave potatorum<\/i>\n                    byproducts as a source of volatile\n                    <i>\u03b1<\/i>\n                    \u2010glucosidase inhibitors"],"prefix":"10.1002","volume":"106","author":[{"given":"Elia\u2010Donaj\u00ed","family":"Ju\u00e1rez\u2010Ni\u00f1o","sequence":"first","affiliation":[{"name":"Instituto Polit\u00e9cnico Nacional, CIIDIR, Unidad Oaxaca  Oaxaca Mexico"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0003-4207-4377","authenticated-orcid":false,"given":"Ang\u00e9lica","family":"Cruz\u2010G\u00f3mez","sequence":"additional","affiliation":[{"name":"Instituto Polit\u00e9cnico Nacional, CIIDIR, Unidad Oaxaca  Oaxaca Mexico"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Rosa","family":"Santillan","sequence":"additional","affiliation":[{"name":"Centro de Investigaci\u00f3n y de Estudios Avanzados del Instituto Polit\u00e9cnico Nacional Departamento de Qu\u00edmica  Ciudad de Mexico Mexico"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Mar\u00eda Eugenia","family":"Ochoa\u2010Becerra","sequence":"additional","affiliation":[{"name":"Centro de Investigaci\u00f3n y de Estudios Avanzados del Instituto Polit\u00e9cnico Nacional Departamento de Qu\u00edmica  Ciudad de Mexico Mexico"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"ORCID":"https:\/\/orcid.org\/0000-0002-6302-5956","authenticated-orcid":false,"given":"Delia","family":"Soto\u2010Castro","sequence":"additional","affiliation":[{"name":"SECIHTI \u2010 Instituto Polit\u00e9cnico Nacional, CIIDIR Unidad Oaxaca  Oaxaca Mexico"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2026,6,15]]},"reference":[{"key":"e_1_2_10_2_1","unstructured":"WHO. 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