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Twenty\u2010nine samples of water were collected directly in the inlet and outlet of the washing machines of three olive mills at various locations in Spain. Preconcentration and clean\u2010up were performed by elution of the pesticides from a C<jats:sub>18<\/jats:sub> SPE cartridge using dichloromethane. The target compounds were determined in the final extract by GC\u2010MS\/MS. The most frequently encountered pesticide residues were terbuthylazine, simazine, and diuron. 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