{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,10,20]],"date-time":"2025-10-20T15:51:49Z","timestamp":1760975509535,"version":"build-2065373602"},"reference-count":29,"publisher":"Wiley","issue":"12","license":[{"start":{"date-parts":[[2007,7,3]],"date-time":"2007-07-03T00:00:00Z","timestamp":1183420800000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2007,8]]},"abstract":"<jats:title>Abstract<\/jats:title><jats:p>A rapid and sensitive method for the determination of 4\u2010fluoro\u20103\u2010phenoxybenzaldehyde cyanohydrin (FPBC) and 4\u2010fluoro\u20103\u2010phenoxy\u2010benzaldehyde (FPB) in honey samples using ultrasonically assisted extraction and gas chromatography with electron capture detection (GC\u2013ECD) has been developed. The different factors affecting the efficiency of the extraction were carefully optimized. The honey sample was extracted with a mixture of hexane and dichloromethane (v\/v, 1:1) utilizing the ultrasonically assisted technique and cleaned up by solid\u2010phase extraction on Oasis HLB cartridges. The eluate was evaporated to dryness and residues were reconstituted to 1.0 mL with hexane and determined by GC\u2013ECD. The calibration curves of fortified samples showed acceptable linear response (<jats:italic>R<\/jats:italic><jats:sup>2<\/jats:sup> &gt;0.99) over a range of 3\u2013100 ng\/g for FPBC and FPB in seven replicate determinations of six concentrations, respectively, and analysis of variance (ANOVA) with a lack\u2010of\u2010fit test was performed to validate the regression data. Overall average recoveries ranged from 90.9 to 106.2% for honey samples. The detection limits were 0.9 ng\/g for FPBC and 1.0 ng\/g for FPB, respectively. 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