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LiChrolut\u2010EN SPE cartridges were used and the optimised analytical conditions were: 7 g of TBV diluted 1:4, 5 mL of washing water, and elution with 10 mL of dichloromethane. The linear ranges and detection and quantitation limits were adequate for the analysis of the studied compounds in TBV. The accuracy of the method was also studied: recoveries up to 80% and repeatability values lower than 15% were obtained for the majority of the studied compounds. Two TBVs of different age were analysed by the optimised method.<\/jats:p>","DOI":"10.1002\/jssc.200800307","type":"journal-article","created":{"date-parts":[[2008,9,10]],"date-time":"2008-09-10T08:33:32Z","timestamp":1221035612000},"page":"3030-3036","source":"Crossref","is-referenced-by-count":50,"title":["Solid\u2010phase extraction method for determination of volatile compounds in traditional balsamic vinegar"],"prefix":"10.1002","volume":"31","author":[{"given":"Enrique","family":"Dur\u00e1n Guerrero","sequence":"first","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Fabio","family":"Chinnici","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Nadia","family":"Natali","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Ram\u00f3n Natera","family":"Mar\u00edn","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Claudio","family":"Riponi","sequence":"additional","affiliation":[],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2008,9,10]]},"reference":[{"key":"e_1_2_1_2_2","doi-asserted-by":"publisher","DOI":"10.1021\/jf020155l"},{"key":"e_1_2_1_3_2","doi-asserted-by":"publisher","DOI":"10.1016\/j.jfca.2004.10.008"},{"key":"e_1_2_1_4_2","doi-asserted-by":"publisher","DOI":"10.1093\/chromsci\/41.6.305"},{"key":"e_1_2_1_5_2","doi-asserted-by":"publisher","DOI":"10.1016\/j.fm.2006.01.006"},{"key":"e_1_2_1_6_2","doi-asserted-by":"publisher","DOI":"10.1111\/j.1365-2672.2006.02906.x"},{"key":"e_1_2_1_7_2","doi-asserted-by":"crossref","first-page":"714","DOI":"10.1093\/jaoac\/77.3.714","volume":"77","author":"Corradini F.","year":"1994","journal-title":"J. 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