{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,9,26]],"date-time":"2026-09-26T03:34:27Z","timestamp":1790393667708,"version":"4.1.0"},"reference-count":31,"publisher":"Wiley","issue":"20","license":[{"start":{"date-parts":[[2012,10,12]],"date-time":"2012-10-12T00:00:00Z","timestamp":1350000000000},"content-version":"vor","delay-in-days":11,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2012,10]]},"abstract":"<jats:p>Two methods based on liquid chromatography\u2013tandem mass spectrometry were developed for the determination of ten aminoglycosides (streptomycin, dihydrostreptomycin, spectinomycin, apramycin, paromomycin, kanamycin A, gentamycin C1, gentamycin C2\/C2a, gentamycin C1a, and neomycin B) in kidney samples from food\u2010producing animals and in honey samples. The methods involved extraction with an aqueous solution (for the kidney samples) or sample dissolution in water (for the honey samples), solid\u2010phase extraction with a weak cation exchange cartridge and injection of the eluate into a liquid chromatography\u2013tandem mass spectrometry system. A zwitterionic hydrophilic interaction chromatography column was used for separation of aminoglycosides and a triple quadrupole mass analyzer was used for detection. The methods were validated according to Decision 2002\/657\/EC. The limits of quantitation ranged from 2 to 125 \u03bcg\/kg in honey and 25 to 264 \u03bcg\/kg in the kidney samples. Interday precision (RSD%) ranged from 6 to 26% in honey and 2 to 21% in kidney. Trueness, expressed as the percentage of error, ranged from 7 to 20% in honey and 1 to 11% in kidney.<\/jats:p>","DOI":"10.1002\/jssc.201200344","type":"journal-article","created":{"date-parts":[[2012,10,12]],"date-time":"2012-10-12T07:55:12Z","timestamp":1350028512000},"page":"2710-2717","source":"Crossref","is-referenced-by-count":47,"title":["Determination of aminoglycoside residues in kidney and honey samples by hydrophilic interaction chromatography\u2010tandem mass spectrometry"],"prefix":"10.1002","volume":"35","author":[{"given":"Praveen","family":"Kumar","sequence":"first","affiliation":[{"name":"Departament de Qu\u00edmica Anal\u00edtica Universitat de Barcelona  Barcelona Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Antoni","family":"R\u00fabies","sequence":"additional","affiliation":[{"name":"Laboratori Ag\u00e8ncia Salut P\u00fablica de Barcelona  Barcelona Spain"},{"name":"CIBER of Epidemiology and Public Health (CIBERESP)  Madrid Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Ramon","family":"Company\u00f3","sequence":"additional","affiliation":[{"name":"Departament de Qu\u00edmica Anal\u00edtica Universitat de Barcelona  Barcelona Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Francesc","family":"Centrich","sequence":"additional","affiliation":[{"name":"Laboratori Ag\u00e8ncia Salut P\u00fablica de Barcelona  Barcelona Spain"},{"name":"CIBER of Epidemiology and Public Health (CIBERESP)  Madrid Spain"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2012,10,12]]},"reference":[{"key":"e_1_2_7_2_1","doi-asserted-by":"publisher","DOI":"10.1002\/9781118067208"},{"key":"e_1_2_7_3_1","first-page":"149","volume":"38","author":"Mutinelli F.","year":"2003","journal-title":"Apiacta"},{"key":"e_1_2_7_4_1","doi-asserted-by":"publisher","DOI":"10.1051\/apido:2005043"},{"key":"e_1_2_7_5_1","first-page":"1","volume":"15","year":"2010","journal-title":"Off. 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