{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2025,10,20]],"date-time":"2025-10-20T00:24:55Z","timestamp":1760919895141,"version":"build-2065373602"},"reference-count":16,"publisher":"Wiley","issue":"4","license":[{"start":{"date-parts":[[2013,1,22]],"date-time":"2013-01-22T00:00:00Z","timestamp":1358812800000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2013,2]]},"abstract":"<jats:p>The aim of this study was to find if fast microwave\u2010assisted extraction could be an alternative to the conventional <jats:styled-content style=\"fixed-case\">S<\/jats:styled-content>oxhlet extraction for the quantification of rotenone in yam bean seeds by <jats:styled-content style=\"fixed-case\">SPE<\/jats:styled-content> and <jats:styled-content style=\"fixed-case\">HPLC<\/jats:styled-content>\u2010<jats:styled-content style=\"fixed-case\">UV<\/jats:styled-content>. For this purpose, an experimental design was used to determine the optimal conditions of the microwave extraction. Then the values of the quantification on three accessions from two different species of yam bean seeds were compared using the two different kinds of extraction. A microwave extraction of 11 min at 55\u00b0C using methanol\/dichloromethane (50:50) allowed rotenone extraction either equivalently or more efficiently than the 8\u2010h\u2010Soxhlet extraction method and was less sensitive to moisture content. The selectivity, precision, trueness, accuracy, and limit of quantification of the method with microwave extraction were also demonstrated.<\/jats:p>","DOI":"10.1002\/jssc.201200347","type":"journal-article","created":{"date-parts":[[2012,11,18]],"date-time":"2012-11-18T20:22:36Z","timestamp":1353270156000},"page":"758-763","source":"Crossref","is-referenced-by-count":8,"title":["Fast microwave\u2010assisted extraction of rotenone for its quantification in seeds of yam bean (<i><scp>P<\/scp>achyrhizus<\/i> sp.)"],"prefix":"10.1002","volume":"36","author":[{"given":"Emmanuelle","family":"Lauti\u00e9","sequence":"first","affiliation":[{"name":"Laboratoire de Pharmacognosie, LDRI Universit\u00e9 Catholique de Louvain  Brussels Belgium"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Catherine","family":"Rasse","sequence":"additional","affiliation":[{"name":"Plateforme technologique de Support en M\u00e9thodologie et Calcul Statistique (SMCS), IMAQ Universit\u00e9 Catholique de Louvain  Brussels Belgium"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Eric","family":"Rozet","sequence":"additional","affiliation":[{"name":"Laboratoire de Chimie analytique, CIRM Universit\u00e9 de Li\u00e8ge  Liege Belgium"},{"name":"F.R.S.\u2010FNRS  Liege Belgium"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Claire","family":"Mourgues","sequence":"additional","affiliation":[{"name":"Laboratoire de Pharmacognosie, LDRI Universit\u00e9 Catholique de Louvain  Brussels Belgium"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Jean\u2010Paul","family":"Vanhelleputte","sequence":"additional","affiliation":[{"name":"Laboratoire de Pharmacognosie, LDRI Universit\u00e9 Catholique de Louvain  Brussels Belgium"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Jo\u00eblle","family":"Quetin\u2010Leclercq","sequence":"additional","affiliation":[{"name":"Laboratoire de Pharmacognosie, LDRI Universit\u00e9 Catholique de Louvain  Brussels Belgium"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2013,1,22]]},"reference":[{"doi-asserted-by":"publisher","key":"e_1_2_7_2_1","DOI":"10.1016\/S0926-6690(02)00056-0"},{"doi-asserted-by":"publisher","key":"e_1_2_7_3_1","DOI":"10.1111\/j.1365-2621.2009.02125.x"},{"doi-asserted-by":"publisher","key":"e_1_2_7_4_1","DOI":"10.1016\/j.foodchem.2010.12.053"},{"doi-asserted-by":"publisher","key":"e_1_2_7_5_1","DOI":"10.1002\/star.200600596"},{"doi-asserted-by":"publisher","key":"e_1_2_7_6_1","DOI":"10.1007\/s11746-999-0144-x"},{"doi-asserted-by":"publisher","key":"e_1_2_7_7_1","DOI":"10.1016\/j.foodchem.2011.09.125"},{"doi-asserted-by":"publisher","key":"e_1_2_7_8_1","DOI":"10.1016\/j.chroma.2006.05.075"},{"doi-asserted-by":"publisher","key":"e_1_2_7_9_1","DOI":"10.1016\/j.supflu.2006.12.021"},{"doi-asserted-by":"publisher","key":"e_1_2_7_10_1","DOI":"10.1016\/j.chroma.2006.05.032"},{"doi-asserted-by":"publisher","key":"e_1_2_7_11_1","DOI":"10.1016\/j.chroma.2007.03.112"},{"doi-asserted-by":"publisher","key":"e_1_2_7_12_1","DOI":"10.1016\/j.aca.2007.02.010"},{"doi-asserted-by":"publisher","key":"e_1_2_7_13_1","DOI":"10.1016\/j.biortech.2009.11.039"},{"doi-asserted-by":"publisher","key":"e_1_2_7_14_1","DOI":"10.1007\/BF01068419"},{"doi-asserted-by":"publisher","key":"e_1_2_7_15_1","DOI":"10.1093\/chromsci\/38.4.174"},{"doi-asserted-by":"publisher","key":"e_1_2_7_16_1","DOI":"10.1016\/S0140-6736(86)90837-8"},{"doi-asserted-by":"publisher","key":"e_1_2_7_17_1","DOI":"10.1016\/S0021-9673(03)01178-6"}],"container-title":["Journal of Separation Science"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/api.wiley.com\/onlinelibrary\/tdm\/v1\/articles\/10.1002%2Fjssc.201200347","content-type":"unspecified","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/analyticalsciencejournals.onlinelibrary.wiley.com\/doi\/pdf\/10.1002\/jssc.201200347","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2025,10,19]],"date-time":"2025-10-19T09:41:42Z","timestamp":1760866902000},"score":1,"resource":{"primary":{"URL":"https:\/\/analyticalsciencejournals.onlinelibrary.wiley.com\/doi\/10.1002\/jssc.201200347"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2013,1,22]]},"references-count":16,"journal-issue":{"issue":"4","published-print":{"date-parts":[[2013,2]]}},"alternative-id":["10.1002\/jssc.201200347"],"URL":"https:\/\/doi.org\/10.1002\/jssc.201200347","archive":["Portico"],"relation":{},"ISSN":["1615-9306","1615-9314"],"issn-type":[{"type":"print","value":"1615-9306"},{"type":"electronic","value":"1615-9314"}],"subject":[],"published":{"date-parts":[[2013,1,22]]}}}