{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,5,9]],"date-time":"2026-05-09T09:39:30Z","timestamp":1778319570872,"version":"3.51.4"},"reference-count":27,"publisher":"Wiley","issue":"11","license":[{"start":{"date-parts":[[2013,4,27]],"date-time":"2013-04-27T00:00:00Z","timestamp":1367020800000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2013,6]]},"abstract":"<jats:p>Metal deactivator additives (<jats:styled-content style=\"fixed-case\">MDA<\/jats:styled-content>s) have been used for over 60 years to prevent metal catalyzed reactions in petroleum products; a commonly used metal deactivator is <jats:italic><jats:styled-content style=\"fixed-case\">N<\/jats:styled-content><\/jats:italic>,<jats:italic><jats:styled-content style=\"fixed-case\">N<\/jats:styled-content><\/jats:italic>\u2032\u2010disalicylidene\u20101,2\u2010propanediamine. The quantitation of low <jats:styled-content style=\"fixed-case\">MDA<\/jats:styled-content> concentrations in fuels is challenging due to the complexity of the sample matrix. In this work, this difficulty was overcome using <jats:styled-content style=\"fixed-case\">GC<\/jats:styled-content> \u00d7 <jats:styled-content style=\"fixed-case\">GC<\/jats:styled-content> hyphenated with a nitrogen chemiluminescence detector. The high resolution power of <jats:styled-content style=\"fixed-case\">GC<\/jats:styled-content> \u00d7 <jats:styled-content style=\"fixed-case\">GC<\/jats:styled-content> avoided co\u2010elution between the <jats:styled-content style=\"fixed-case\">MDA<\/jats:styled-content> and other sample matrix compounds; while the enhanced sensitivity of <jats:styled-content style=\"fixed-case\">GC<\/jats:styled-content> \u00d7 <jats:styled-content style=\"fixed-case\">GC<\/jats:styled-content> and the use of a nitrogen chemiluminescence detector supplied a high sensitivity and specificity for nitrogen compounds. For the analysis, the <jats:styled-content style=\"fixed-case\">MDA<\/jats:styled-content> additive was derivatized with the silylation agent <jats:italic><jats:styled-content style=\"fixed-case\">N<\/jats:styled-content><\/jats:italic>,<jats:styled-content style=\"fixed-case\">O<\/jats:styled-content>\u2010bis (trimethylsilyl)trifluoroacetamide at room temperature and its quantitation was based on an external calibration curve; good linear response was obtained in the 1.4\u20138.6 ppm range.<\/jats:p>","DOI":"10.1002\/jssc.201300050","type":"journal-article","created":{"date-parts":[[2013,3,14]],"date-time":"2013-03-14T04:03:42Z","timestamp":1363233822000},"page":"1768-1763","source":"Crossref","is-referenced-by-count":11,"title":["Quantitation method of <i>N<\/i>,<i>N<\/i> \u2032\u2010disalicylidene\u20101,2\u2010propanediamine by comprehensive two\u2010dimensional gas chromatography coupled to a nitrogen chemiluminescence detector"],"prefix":"10.1002","volume":"36","author":[{"given":"Kristina","family":"Lissitsyna","sequence":"first","affiliation":[{"name":"Universidad Complutense de Madrid Departamento de Qu\u00edmica Anal\u00edtica  Madrid Spain"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Sonia","family":"Huertas","sequence":"additional","affiliation":[{"name":"Centro Tecnol\u00f3gico de Repsol  Madrid Spain"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Luis Carlos","family":"Quintero","sequence":"additional","affiliation":[{"name":"Centro Tecnol\u00f3gico de Repsol  Madrid Spain"}],"role":[{"role":"author","vocabulary":"crossref"}]},{"given":"Luis Maria","family":"Polo","sequence":"additional","affiliation":[{"name":"Universidad Complutense de Madrid Departamento de Qu\u00edmica Anal\u00edtica  Madrid Spain"}],"role":[{"role":"author","vocabulary":"crossref"}]}],"member":"311","published-online":{"date-parts":[[2013,4,27]]},"reference":[{"key":"e_1_2_6_2_1","doi-asserted-by":"publisher","DOI":"10.1021\/ef00025a001"},{"key":"e_1_2_6_3_1","doi-asserted-by":"publisher","DOI":"10.1021\/ef970096r"},{"key":"e_1_2_6_4_1","doi-asserted-by":"publisher","DOI":"10.1021\/ef010113j"},{"key":"e_1_2_6_5_1","doi-asserted-by":"publisher","DOI":"10.1115\/1.2817061"},{"key":"e_1_2_6_6_1","doi-asserted-by":"publisher","DOI":"10.1093\/chromsci\/38.9.393"},{"key":"e_1_2_6_7_1","doi-asserted-by":"publisher","DOI":"10.1093\/chromsci\/29.6.227"},{"key":"e_1_2_6_8_1","doi-asserted-by":"publisher","DOI":"10.1093\/chromsci\/40.5.276"},{"key":"e_1_2_6_9_1","doi-asserted-by":"publisher","DOI":"10.1002\/(SICI)1521-4168(19991201)22:12<647::AID-JHRC647>3.0.CO;2-V"},{"key":"e_1_2_6_10_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0165-9936(02)00814-2"},{"key":"e_1_2_6_11_1","doi-asserted-by":"publisher","DOI":"10.1002\/1615-9314(20020301)25:4<201::AID-JSSC201>3.0.CO;2-B"},{"key":"e_1_2_6_12_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2008.01.002"},{"key":"e_1_2_6_13_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0021-9673(03)00242-5"},{"key":"e_1_2_6_14_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0021-9673(01)00785-3"},{"key":"e_1_2_6_15_1","doi-asserted-by":"publisher","DOI":"10.1002\/(SICI)1521-4168(19990401)22:4<235::AID-JHRC235>3.0.CO;2-R"},{"key":"e_1_2_6_16_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0021-9673(03)01237-8"},{"key":"e_1_2_6_17_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0021-9673(02)00327-8"},{"key":"e_1_2_6_18_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2006.10.014"},{"key":"e_1_2_6_19_1","doi-asserted-by":"publisher","DOI":"10.1016\/S0021-9673(03)01301-3"},{"key":"e_1_2_6_20_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2003.08.048"},{"key":"e_1_2_6_21_1","doi-asserted-by":"publisher","DOI":"10.1002\/(SICI)1521-4168(20000301)23:3<197::AID-JHRC197>3.0.CO;2-R"},{"key":"e_1_2_6_22_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2011.05.009"},{"key":"e_1_2_6_23_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.forsciint.2004.02.042"},{"key":"e_1_2_6_24_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2005.05.106"},{"key":"e_1_2_6_25_1","doi-asserted-by":"publisher","DOI":"10.1002\/jssc.200301643"},{"key":"e_1_2_6_26_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2007.01.142"},{"key":"e_1_2_6_27_1","doi-asserted-by":"publisher","DOI":"10.1002\/9783527625215"},{"key":"e_1_2_6_28_1","doi-asserted-by":"publisher","DOI":"10.2516\/ogst:2007004"}],"container-title":["Journal of Separation Science"],"original-title":[],"language":"en","link":[{"URL":"https:\/\/api.wiley.com\/onlinelibrary\/tdm\/v1\/articles\/10.1002%2Fjssc.201300050","content-type":"unspecified","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/api.wiley.com\/onlinelibrary\/tdm\/v1\/articles\/10.1002%2Fjssc.201300050","content-type":"application\/pdf","content-version":"vor","intended-application":"text-mining"},{"URL":"https:\/\/analyticalsciencejournals.onlinelibrary.wiley.com\/doi\/pdf\/10.1002\/jssc.201300050","content-type":"unspecified","content-version":"vor","intended-application":"similarity-checking"}],"deposited":{"date-parts":[[2025,10,19]],"date-time":"2025-10-19T09:16:06Z","timestamp":1760865366000},"score":1,"resource":{"primary":{"URL":"https:\/\/analyticalsciencejournals.onlinelibrary.wiley.com\/doi\/10.1002\/jssc.201300050"}},"subtitle":[],"short-title":[],"issued":{"date-parts":[[2013,4,27]]},"references-count":27,"journal-issue":{"issue":"11","published-print":{"date-parts":[[2013,6]]}},"alternative-id":["10.1002\/jssc.201300050"],"URL":"https:\/\/doi.org\/10.1002\/jssc.201300050","archive":["Portico"],"relation":{},"ISSN":["1615-9306","1615-9314"],"issn-type":[{"value":"1615-9306","type":"print"},{"value":"1615-9314","type":"electronic"}],"subject":[],"published":{"date-parts":[[2013,4,27]]}}}