{"status":"ok","message-type":"work","message-version":"1.0.0","message":{"indexed":{"date-parts":[[2026,9,14]],"date-time":"2026-09-14T06:15:01Z","timestamp":1789366501217,"version":"build-2803163510"},"reference-count":26,"publisher":"Wiley","issue":"20","license":[{"start":{"date-parts":[[2013,9,4]],"date-time":"2013-09-04T00:00:00Z","timestamp":1378252800000},"content-version":"vor","delay-in-days":0,"URL":"http:\/\/onlinelibrary.wiley.com\/termsAndConditions#vor"}],"funder":[{"name":"Central Institute for Labour Protection-National Research Institute"}],"content-domain":{"domain":[],"crossmark-restriction":false},"short-container-title":["J of Separation Science"],"published-print":{"date-parts":[[2013,10]]},"abstract":"<jats:p>A needle\u2010trap device, with immobilized sorbent inside the syringe, coupled with <jats:styled-content style=\"fixed-case\">GC<\/jats:styled-content>\u2013<jats:styled-content style=\"fixed-case\">MS<\/jats:styled-content> was applied for air sampling and determination of chlorinated volatile organic compounds such as dichloromethane, trichloromethane, and tetrachloromethane. The application of a needle trap packed with combination of three sorbents including Tenax <jats:styled-content style=\"fixed-case\">TA<\/jats:styled-content>, <jats:styled-content style=\"fixed-case\">C<\/jats:styled-content>arbopack <jats:styled-content style=\"fixed-case\">X<\/jats:styled-content>, and <jats:styled-content style=\"fixed-case\">C<\/jats:styled-content>arboxen 1000 resulted in detection limits of few pg for chlorinated volatile compounds and recoveries of 99.2\u2013102.8%. The extraction and desorption parameters were optimized within the study. As a result, the precision determined as <jats:styled-content style=\"fixed-case\">RSD<\/jats:styled-content> was equal to 5.05 and 3.03 and 6.52% for dichloromethane, trichloromethane, and tetrachloromethane, respectively. The storage time for chlorinated compounds up to 48 h and reusability of the needle\u2010trap device were verified. The obtained results have proved the ability of needle traps to compete with other solventless sampling and sample preparation extraction techniques.<\/jats:p>","DOI":"10.1002\/jssc.201300571","type":"journal-article","created":{"date-parts":[[2013,8,19]],"date-time":"2013-08-19T03:26:43Z","timestamp":1376882803000},"page":"3372-3378","source":"Crossref","is-referenced-by-count":19,"title":["Needle\u2010trap device for the sampling and determination of chlorinated volatile compounds"],"prefix":"10.1002","volume":"36","author":[{"given":"El\u017cbieta","family":"Dobrzy\u0144ska","sequence":"first","affiliation":[{"name":"Department of Chemical, Aerosol and Biological Hazards Central Institute for Labour Protection\u2014National Research Institute  Warsaw Poland"},{"name":"Department of Environmental Chemistry and Bioanalytics Faculty of Chemistry, Nicolaus Copernicus University  Toru\u0144 Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]},{"given":"Bogus\u0142aw","family":"Buszewski","sequence":"additional","affiliation":[{"name":"Department of Environmental Chemistry and Bioanalytics Faculty of Chemistry, Nicolaus Copernicus University  Toru\u0144 Poland"}],"role":[{"vocabulary":"crossref","role":"author"}]}],"member":"311","published-online":{"date-parts":[[2013,9,4]]},"reference":[{"key":"e_1_2_7_2_1","first-page":"478","volume":"32","author":"Raschdorf F.","year":"1978","journal-title":"Chimia"},{"key":"e_1_2_7_3_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.chroma.2008.02.090"},{"key":"e_1_2_7_4_1","doi-asserted-by":"publisher","DOI":"10.1016\/j.aca.2010.06.020"},{"key":"e_1_2_7_5_1","doi-asserted-by":"crossref","first-page":"387","DOI":"10.4209\/aaqr.2011.01.0001","volume":"11","author":"Cheng W.\u2010H.","year":"2011","journal-title":"Aerosol Air Qual. 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